benzyl 2-deoxy-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

Base Information

Chemical Name:benzyl 2-deoxy-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside
CAS No.:1055335-23-3
Molecular Formula:C₁₆H₂₀Cl₃NO₇
Molecular Weight:444.696
Hs Code.:

Synonyms:benzyl 2-deoxy-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

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Chemical Property of benzyl 2-deoxy-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

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Technology Process of benzyl 2-deoxy-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

There total 3 articles about benzyl 2-deoxy-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 133940-44-0,133940-45-1
benzyl 3,4,6-tri-O-acetyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranoside

: 1055335-23-3
benzyl 2-deoxy-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

Guidance literature:: benzyl 3,4,6-tri-O-acetyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranoside; With sodium methylate; In methanol; at -5 ℃; for 2.5h;

In methanol;
DOI:10.1007/s10719-018-9839-2

Reference yield:

: 187022-49-7
(2R,3S,4R,5R,6S)-2-(acetoxymethyl)-6-(phenylthio)-5-(((2,2,2-trichloroethoxy)carbonyl)amino)tetrahydro-2H-pyran-3,4-diyl diacetate

: 1055335-23-3
benzyl 2-deoxy-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-iodo-succinimide / dichloromethane / 23 h / -10 °C / Molecular sieve

2.1: sodium methylate / methanol / 2.5 h / -5 °C

2.2: Amberlite IRC-50 H+ resin

With N-iodo-succinimide; sodium methylate; In methanol; dichloromethane;
DOI:10.1007/s10719-018-9839-2

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 1055335-23-3
benzyl 2-deoxy-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-iodo-succinimide / dichloromethane / 23 h / -10 °C / Molecular sieve

2.1: sodium methylate / methanol / 2.5 h / -5 °C

2.2: Amberlite IRC-50 H+ resin

With N-iodo-succinimide; sodium methylate; In methanol; dichloromethane;
DOI:10.1007/s10719-018-9839-2