2-3',4'-dimethoxy-2'-methoxycarbonylphenyl-2,3-epoxy-2,3-dihydro-6,7-methylenedioxy-1,4-naphthoquinone

Base Information

Chemical Name:2-3',4'-dimethoxy-2'-methoxycarbonylphenyl-2,3-epoxy-2,3-dihydro-6,7-methylenedioxy-1,4-naphthoquinone
CAS No.:82464-07-1
Molecular Formula:C₂₁H₁₆O₉
Molecular Weight:412.353
Hs Code.:

Synonyms:2-3',4'-dimethoxy-2'-methoxycarbonylphenyl-2,3-epoxy-2,3-dihydro-6,7-methylenedioxy-1,4-naphthoquinone

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Chemical Property of 2-3',4'-dimethoxy-2'-methoxycarbonylphenyl-2,3-epoxy-2,3-dihydro-6,7-methylenedioxy-1,4-naphthoquinone

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Technology Process of 2-3',4'-dimethoxy-2'-methoxycarbonylphenyl-2,3-epoxy-2,3-dihydro-6,7-methylenedioxy-1,4-naphthoquinone

There total 5 articles about 2-3',4'-dimethoxy-2'-methoxycarbonylphenyl-2,3-epoxy-2,3-dihydro-6,7-methylenedioxy-1,4-naphthoquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 82464-08-2
2-3',4'-dimethoxy-2'-methoxycarbonylphenyl-2,3-epoxy-1,2,3,4-tetrahydro-6,7-methylenedioxy-1-oxo-4-phenyliminonaphthalene

: 82464-07-1
2-3',4'-dimethoxy-2'-methoxycarbonylphenyl-2,3-epoxy-2,3-dihydro-6,7-methylenedioxy-1,4-naphthoquinone

Guidance literature:: With hydrogenchloride; In methanol; for 0.5h; Ambient temperature;
DOI:10.1248/cpb.30.569

Reference yield: 90.0%

: 82464-06-0
2-3',4'-dimethoxy-2'-methoxycarbonylphenyl-6,7-methylenedioxy-1,4-naphthoquinone

: 82464-07-1
2-3',4'-dimethoxy-2'-methoxycarbonylphenyl-2,3-epoxy-2,3-dihydro-6,7-methylenedioxy-1,4-naphthoquinone

Guidance literature:: With tert.-butylhydroperoxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In benzene; for 24h; Ambient temperature;
DOI:10.1248/cpb.30.569

Reference yield:

: 67258-01-9,82534-85-8
4b,10bβ,11,12-tetrahydro-4bβ,12β-(N-phenylepoxyimino)oxychelerythrine

: 82464-07-1
2-3',4'-dimethoxy-2'-methoxycarbonylphenyl-2,3-epoxy-2,3-dihydro-6,7-methylenedioxy-1,4-naphthoquinone

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / H₂ / 10percent Pd-C / methanol / 0.25 h / Ambient temperature

3: 99 percent / 10percent HCl / methanol / 0.5 h / Ambient temperature

4: 90 percent / tert-butyl hydroperoxide, DBU / benzene / 24 h / Ambient temperature

With hydrogenchloride; tert.-butylhydroperoxide; hydrogen; 1,8-diazabicyclo[5.4.0]undec-7-ene; palladium on activated charcoal; In methanol; benzene;
DOI:10.1248/cpb.30.569