N-<3-(tert-butoxycarbonyl)-6-methylphenyl>-2,2-dibromopropanoic acid amide

Base Information

Chemical Name:N-<3-(tert-butoxycarbonyl)-6-methylphenyl>-2,2-dibromopropanoic acid amide
CAS No.:111773-29-6
Molecular Formula:C₁₅H₁₉Br₂NO₃
Molecular Weight:421.129
Hs Code.:

Synonyms:N-<3-(tert-butoxycarbonyl)-6-methylphenyl>-2,2-dibromopropanoic acid amide

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Chemical Property of N-<3-(tert-butoxycarbonyl)-6-methylphenyl>-2,2-dibromopropanoic acid amide

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Technology Process of N-<3-(tert-butoxycarbonyl)-6-methylphenyl>-2,2-dibromopropanoic acid amide

There total 1 articles about N-<3-(tert-butoxycarbonyl)-6-methylphenyl>-2,2-dibromopropanoic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 18791-02-1
2,3-dibromo-propionyl chloride

: 111773-25-2
tert-butyl 3-amino-4-methylbenzoate

: 111773-30-9
N-<3-(tert-butoxycarbonyl)-6-methylphenyl>-2-bromo-2-propenoic acid ami

: 111773-29-6
N-<3-(tert-butoxycarbonyl)-6-methylphenyl>-2,2-dibromopropanoic acid amide

Guidance literature:: With 2,3-Lutidine; In toluene; at 20 ℃; for 0.5h;
DOI:10.1021/jm00397a018

Reference yield: 24.0%

: 111773-29-6
N-<3-(tert-butoxycarbonyl)-6-methylphenyl>-2,2-dibromopropanoic acid amide

: 111793-84-1
N-<3-(tert-butoxycarbonyl)-6-methylphenyl>-3-bromoazetidin-2-one

Guidance literature:: With sodium hydride; In dichloromethane; N,N-dimethyl-formamide; for 2h;
DOI:10.1021/jm00397a018

Reference yield:

: 111773-29-6
N-<3-(tert-butoxycarbonyl)-6-methylphenyl>-2,2-dibromopropanoic acid amide

: 111773-37-6
N-(3-carboxy-6-methylphenyl)-3-bromoazetidin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 24 percent / NaH / dimethylformamide; CH₂Cl₂ / 2 h

2: 92 percent / CF₃CO₂H / CH₂Cl₂ / 1 h / 10 °C

With sodium hydride; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00397a018