2-(3,5-di-tert-butylphenyl)pyrrole

Base Information

Chemical Name:2-(3,5-di-tert-butylphenyl)pyrrole
CAS No.:1261292-10-7
Molecular Formula:C₁₈H₂₅N
Molecular Weight:255.403
Hs Code.:

Synonyms:2-(3,5-di-tert-butylphenyl)pyrrole

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Chemical Property of 2-(3,5-di-tert-butylphenyl)pyrrole

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Technology Process of 2-(3,5-di-tert-butylphenyl)pyrrole

There total 2 articles about 2-(3,5-di-tert-butylphenyl)pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1261292-09-4
C₂₃H₃₃NO₂

: 1261292-10-7
2-(3,5-di-tert-butylphenyl)pyrrole

Guidance literature:: With sodium methylate; In tetrahydrofuran; methanol; at 25 ℃; for 15h;
DOI:10.1002/chem.201100619

Reference yield:

: 197223-39-5
3,5-di-tert-butylphenyl boronic acid

: 1261292-10-7
2-(3,5-di-tert-butylphenyl)pyrrole

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-Bromosuccinimide / tetrahydrofuran / 1 h / Inert atmosphere; Darkness

1.2: 24 h / 68 °C / Inert atmosphere

2.1: trifluoroacetic acid / dichloromethane / 1 h / 25 °C / Inert atmosphere; Darkness

With N-Bromosuccinimide; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol102879g

Reference yield: 57.0%

: 1261292-10-7
2-(3,5-di-tert-butylphenyl)pyrrole

: 109-63-7
boron trifluoride diethyl etherate

: 72659-48-4
4-formyl-1,8-dimethoxynaphthalene

: C₄₉H₅₇BF₂N₂O₂

Guidance literature:: 2-(3,5-di-tert-butylphenyl)pyrrole; 4-formyl-1,8-dimethoxynaphthalene; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

boron trifluoride diethyl etherate; With triethylamine; In dichloromethane; for 4h;
DOI:10.1039/c6cc05126j