(3R,11bS)-11-benzyl-11b-methyl-5-oxo-3-phenyl-3,5,6,11b-tetrahydro-2H-oxazolo[3',2':1,2]pyrido[3,4-b]indole

Base Information

Chemical Name:(3R,11bS)-11-benzyl-11b-methyl-5-oxo-3-phenyl-3,5,6,11b-tetrahydro-2H-oxazolo[3',2':1,2]pyrido[3,4-b]indole
CAS No.:1374399-78-6
Molecular Formula:C₂₇H₂₄N₂O₂
Molecular Weight:408.5
Hs Code.:

Synonyms:(3R,11bS)-11-benzyl-11b-methyl-5-oxo-3-phenyl-3,5,6,11b-tetrahydro-2H-oxazolo[3',2':1,2]pyrido[3,4-b]indole

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Chemical Property of (3R,11bS)-11-benzyl-11b-methyl-5-oxo-3-phenyl-3,5,6,11b-tetrahydro-2H-oxazolo[3',2':1,2]pyrido[3,4-b]indole

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Technology Process of (3R,11bS)-11-benzyl-11b-methyl-5-oxo-3-phenyl-3,5,6,11b-tetrahydro-2H-oxazolo[3',2':1,2]pyrido[3,4-b]indole

There total 5 articles about (3R,11bS)-11-benzyl-11b-methyl-5-oxo-3-phenyl-3,5,6,11b-tetrahydro-2H-oxazolo[3',2':1,2]pyrido[3,4-b]indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1374399-76-4
2-acetyl-1-benzyl-3-indoleacetic acid

: 56613-80-0
D-2-phenylglycinol

: 1374399-78-6
(3R,11bS)-11-benzyl-11b-methyl-5-oxo-3-phenyl-3,5,6,11b-tetrahydro-2H-oxazolo[3',2':1,2]pyrido[3,4-b]indole

Guidance literature:: In benzene; for 18h; Reflux;
DOI:10.1002/ejoc.201101718

Reference yield:

: 1384958-13-7
C₂₁H₂₁NO₃

: 1374399-78-6
(3R,11bS)-11-benzyl-11b-methyl-5-oxo-3-phenyl-3,5,6,11b-tetrahydro-2H-oxazolo[3',2':1,2]pyrido[3,4-b]indole

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / ethanol; water / 0.5 h / Reflux

2: benzene / 18 h / Reflux

With sodium hydroxide; In ethanol; water; benzene;
DOI:10.1002/ejoc.201101718

Reference yield:

: 1384957-96-3
C₁₄H₁₅NO₃

: 1374399-78-6
(3R,11bS)-11-benzyl-11b-methyl-5-oxo-3-phenyl-3,5,6,11b-tetrahydro-2H-oxazolo[3',2':1,2]pyrido[3,4-b]indole

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetonitrile / 22 h / 80 °C

2: sodium hydroxide / ethanol; water / 0.5 h / Reflux

3: benzene / 18 h / Reflux

With potassium carbonate; sodium hydroxide; In ethanol; water; acetonitrile; benzene;
DOI:10.1002/ejoc.201101718