C₉H₉N₃OS

Base Information

• Chemical Name: C₉H₉N₃OS
• CAS No.: 1435388-16-1
• Molecular Formula: C₉H₉N₃OS
• Molecular Weight: 207.256
• Mol file: 1435388-16-1.mol

Synonyms:C₉H₉N₃OS

Chemical Property of C₉H₉N₃OS

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₉H₉N₃OS

There total 5 articles about C₉H₉N₃OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

C9H5N3O5S → C9H9N3OS (1435388-16-1)

Guidance literature:

With iron; ammonium chloride; In ethanol; at 80 ℃; for 1h; Inert atmosphere;

DOI:10.1021/jm301793a

Reference yield:

C9H5N3O5S → C9H9N3OS (1435388-16-1)

Guidance literature:

Multi-step reaction with 2 steps

1: sulfuric acid; acetic acid / 1 h / 100 °C / Inert atmosphere

2: iron; ammonium chloride / ethanol / 1 h / 80 °C / Inert atmosphere

With sulfuric acid; iron; ammonium chloride; acetic acid; In ethanol;

DOI:10.1021/jm301793a

Reference yield:

1-(3,5-dinitrophenyl)ethanone (14401-75-3) → C9H9N3OS (1435388-16-1)

Guidance literature:

Multi-step reaction with 4 steps

1: copper(ll) bromide / ethyl acetate / Reflux; Inert atmosphere

2: acetone / 0.5 h / 20 °C / Inert atmosphere

3: sulfuric acid; acetic acid / 1 h / 100 °C / Inert atmosphere

4: iron; ammonium chloride / ethanol / 1 h / 80 °C / Inert atmosphere

With sulfuric acid; iron; ammonium chloride; acetic acid; copper(ll) bromide; In ethanol; ethyl acetate; acetone;

DOI:10.1021/jm301793a

upstream raw materials:

1-(3,5-dinitrophenyl)ethanone

2-bromo-1-(3,5-dinitro-phenyl)-ethanone