iso-2'-C-methyl-2',3'-O-isopropylidene-5'-O-triphenylmethyl-uridine

Base Information

Chemical Name:iso-2'-C-methyl-2',3'-O-isopropylidene-5'-O-triphenylmethyl-uridine
CAS No.:1044589-72-1
Molecular Formula:C₃₂H₃₂N₂O₆
Molecular Weight:540.616
Hs Code.:

Synonyms:iso-2'-C-methyl-2',3'-O-isopropylidene-5'-O-triphenylmethyl-uridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of iso-2'-C-methyl-2',3'-O-isopropylidene-5'-O-triphenylmethyl-uridine

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Technology Process of iso-2'-C-methyl-2',3'-O-isopropylidene-5'-O-triphenylmethyl-uridine

There total 1 articles about iso-2'-C-methyl-2',3'-O-isopropylidene-5'-O-triphenylmethyl-uridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1044589-67-4
(1R,2R,3R)-1-(triphenylmethyloxymethyl)-2,3-O-isopropylidene-3-C-(p-toluenesulfonyloxymethyl)-furan-2,3-diol

: 66-22-8,144104-68-7,18324-22-6,27072-01-1,2920-92-5,51953-19-6
uracil

: 1044589-72-1
iso-2'-C-methyl-2',3'-O-isopropylidene-5'-O-triphenylmethyl-uridine

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 140 ℃; for 24h;
DOI:10.1016/j.tet.2008.05.022

Reference yield: 58.0%

: 1044589-72-1
iso-2'-C-methyl-2',3'-O-isopropylidene-5'-O-triphenylmethyl-uridine

: 1044589-76-5
iso-2'-C-methyl-2',3'-O-isopropylidene-5'-O-triphenylmethyl-cytidine

Guidance literature:: iso-2'-C-methyl-2',3'-O-isopropylidene-5'-O-triphenylmethyl-uridine; With 1-Methylpyrrolidine; trifluoroacetic anhydride; In acetonitrile; for 0.5h;

With 4-nitro-phenol; In acetonitrile; at 0 ℃; for 3h;

With ammonia; In methanol; at 100 ℃; for 5h; Further stages.;
DOI:10.1016/j.tet.2008.05.022