4,6-di-O-benzyl-2,3-dideoxy-D-erythro-hex-2-enopyranosyl-(1->3)-1,2:5,6-di-O-isopropylidene-D-glucofuranoside

Base Information

Chemical Name:4,6-di-O-benzyl-2,3-dideoxy-D-erythro-hex-2-enopyranosyl-(1->3)-1,2:5,6-di-O-isopropylidene-D-glucofuranoside
CAS No.:669082-61-5
Molecular Formula:C₃₂H₄₀O₉
Molecular Weight:568.664
Hs Code.:

Synonyms:4,6-di-O-benzyl-2,3-dideoxy-D-erythro-hex-2-enopyranosyl-(1->3)-1,2:5,6-di-O-isopropylidene-D-glucofuranoside

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Chemical Property of 4,6-di-O-benzyl-2,3-dideoxy-D-erythro-hex-2-enopyranosyl-(1->3)-1,2:5,6-di-O-isopropylidene-D-glucofuranoside

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Technology Process of 4,6-di-O-benzyl-2,3-dideoxy-D-erythro-hex-2-enopyranosyl-(1->3)-1,2:5,6-di-O-isopropylidene-D-glucofuranoside

There total 2 articles about 4,6-di-O-benzyl-2,3-dideoxy-D-erythro-hex-2-enopyranosyl-(1->3)-1,2:5,6-di-O-isopropylidene-D-glucofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 582-52-5
1,2:5,6-di-O-isopropylidene-α-D-glucofuranose

: (2R,3S)-6-(allyloxy)-3-(benzyloxy)-2-((benzyloxy)methyl)-3,6-dihydro-2H-pyran

: 669082-61-5
4,6-di-O-benzyl-2,3-dideoxy-D-erythro-hex-2-enopyranosyl-(1->3)-1,2:5,6-di-O-isopropylidene-D-glucofuranoside

Guidance literature:: With N-Bromosuccinimide; zinc trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 15h;
DOI:10.1021/jo102333x

Reference yield:

: 203630-08-4
1,5-Anhydro-4,6-di-O-benzyl-2-deoxy-D-arabino-hex-1-enitol

: 582-52-5
1,2:5,6-di-O-isopropylidene-α-D-glucofuranose

: 669082-61-5
4,6-di-O-benzyl-2,3-dideoxy-D-erythro-hex-2-enopyranosyl-(1->3)-1,2:5,6-di-O-isopropylidene-D-glucofuranoside

: 669082-53-5
4,6-di-O-benzyl-2,3-dideoxy-D-erythro-hex-2-enopyranosyl-(1->3)-1,2:5,6-di-O-isopropylidene-D-glucofuranoside

Guidance literature:: With indium(III) chloride; In dichloromethane; at 30 ℃; for 8h; optical yield given as %de; Inert atmosphere;
DOI:10.1016/j.tetlet.2009.04.084