C₁₄H₁₈FN₅O₂

Base Information

Chemical Name:C₁₄H₁₈FN₅O₂
CAS No.:1334167-77-9
Molecular Formula:C₁₄H₁₈FN₅O₂
Molecular Weight:307.328
Hs Code.:

C<sub>14</sub>H<sub>18</sub>FN<sub>5</sub>O<sub>2</sub>

Synonyms:C₁₄H₁₈FN₅O₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₁₈FN₅O₂

Chemical Property:

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Technology Process of C₁₄H₁₈FN₅O₂

There total 10 articles about C₁₄H₁₈FN₅O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1334167-81-5
C₁₄H₁₆FN₇O₂

: 1334167-77-9
C₁₄H₁₈FN₅O₂

Guidance literature:: With hydrogen; 10% palladium on charcoal; In methanol; for 1.5h;

Reference yield:

: 509151-97-7
2-(2-fluoro-4-nitrophenylamino)ethanol

: 1334167-77-9
C₁₄H₁₈FN₅O₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: triethylamine / dichloromethane / 0.5 h / 0 °C

2.1: N-ethyl-N,N-diisopropylamine / ethanol; water / 2 h / Reflux

3.1: acetic acid / 15 h / Reflux

3.2: pH 8 - 9

4.1: hydrogen / palladium-on-charcoal / methanol / 4 h / 20 °C

5.1: dichloromethane / 3 h / 20 °C

5.2: 4 h / 50 °C

6.1: lithium tert-butoxide; methanol / N,N-dimethyl-formamide; tetrahydrofuran / 0.5 h / 0 °C

6.2: 10 h / 20 °C

7.1: triphenylphosphine; diphenyl phosphoryl azide; di-isopropyl azodicarboxylate / tetrahydrofuran / 1.5 h / 0 °C

8.1: hydrogen / 10% palladium on charcoal / methanol / 1.5 h

With methanol; di-isopropyl azodicarboxylate; diphenyl phosphoryl azide; hydrogen; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; lithium tert-butoxide; 10% palladium on charcoal; palladium-on-charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 369-34-6
3,4-difluoronitrobenzene

: 1334167-77-9
C₁₄H₁₈FN₅O₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: acetonitrile / 4 h / Reflux

2.1: triethylamine / dichloromethane / 0.5 h / 0 °C

3.1: N-ethyl-N,N-diisopropylamine / ethanol; water / 2 h / Reflux

4.1: acetic acid / 15 h / Reflux

4.2: pH 8 - 9

5.1: hydrogen / palladium-on-charcoal / methanol / 4 h / 20 °C

6.1: dichloromethane / 3 h / 20 °C

6.2: 4 h / 50 °C

7.1: lithium tert-butoxide; methanol / N,N-dimethyl-formamide; tetrahydrofuran / 0.5 h / 0 °C

7.2: 10 h / 20 °C

8.1: triphenylphosphine; diphenyl phosphoryl azide; di-isopropyl azodicarboxylate / tetrahydrofuran / 1.5 h / 0 °C

9.1: hydrogen / 10% palladium on charcoal / methanol / 1.5 h

With methanol; di-isopropyl azodicarboxylate; diphenyl phosphoryl azide; hydrogen; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; lithium tert-butoxide; 10% palladium on charcoal; palladium-on-charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;