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bromodifluoromethylphenylacetylene

Base Information Edit
  • Chemical Name:bromodifluoromethylphenylacetylene
  • CAS No.:82477-43-8
  • Molecular Formula:C9H5BrF2
  • Molecular Weight:231.04
  • Hs Code.:
  • Mol file:82477-43-8.mol
bromodifluoromethylphenylacetylene

Synonyms:bromodifluoromethylphenylacetylene

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Chemical Property of bromodifluoromethylphenylacetylene Edit
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Technology Process of bromodifluoromethylphenylacetylene

There total 6 articles about bromodifluoromethylphenylacetylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
phenylacetylene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;
dibromodifluoromethane; In ethanol; hexane; at -100 - -50 ℃;
DOI:10.1021/ol052816g
Guidance literature:
phenylacetylene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; Inert atmosphere;
(bromodifluoromethyl)diphenylsulfonium trifluoromethanesulfonate; In tetrahydrofuran; hexane; Inert atmosphere; Cooling;
DOI:10.1055/s-0029-1219579
Guidance literature:
With n-butyllithium; Yield given. Multistep reaction. Yields of byproduct given; 2) THF, 1 h, -20 deg C; 1 h, 0 deg C; 4 h, RT;
DOI:10.1016/S0022-1139(00)80063-9
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