3,3'-dideoxy-3,3'-ditosylamino α-D-mannopyranosyl α-D-mannopyranoside 4,6,4',6'-tetraacetate

Base Information

Chemical Name:3,3'-dideoxy-3,3'-ditosylamino α-D-mannopyranosyl α-D-mannopyranoside 4,6,4',6'-tetraacetate
CAS No.:95079-10-0
Molecular Formula:C₃₄H₄₄N₂O₁₇S₂
Molecular Weight:816.859
Hs Code.:

Synonyms:3,3'-dideoxy-3,3'-ditosylamino α-D-mannopyranosyl α-D-mannopyranoside 4,6,4',6'-tetraacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,3'-dideoxy-3,3'-ditosylamino α-D-mannopyranosyl α-D-mannopyranoside 4,6,4',6'-tetraacetate

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Technology Process of 3,3'-dideoxy-3,3'-ditosylamino α-D-mannopyranosyl α-D-mannopyranoside 4,6,4',6'-tetraacetate

There total 2 articles about 3,3'-dideoxy-3,3'-ditosylamino α-D-mannopyranosyl α-D-mannopyranoside 4,6,4',6'-tetraacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.7%

: 95120-32-4
4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranosyl 4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranoside

: 70-55-3
toluene-4-sulfonamide

: 95079-10-0
3,3'-dideoxy-3,3'-ditosylamino α-D-mannopyranosyl α-D-mannopyranoside 4,6,4',6'-tetraacetate

: 95079-08-6
2,2'-dideoxy-2,2'-ditosylamino α-D-mannopyranosyl α-D-mannopyranoside 4,6,4',6'-tetraacetate

: 95079-09-7
2,3'-dideoxy-2,3'-ditosylamino α-D-mannopyranosyl α-D-mannopyranoside 4,6,4',6'-tetraacetate

Guidance literature:: With osmium(VIII) oxide; silver nitrate; In hexane; tert-butyl alcohol; at 40 ℃; for 22h; Yields of byproduct given;
DOI:10.1016/0008-6215(84)85021-1

Reference yield:

: 95120-32-4
4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranosyl 4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranoside

: 70-55-3
toluene-4-sulfonamide

: 95079-12-2
2-deoxy-2-(p-toluenesulfonamido)-α-D-mannopyranosyl 3-deoxy-3-(p-toluenesulfonamido)-α-D-mannopyranoside

: 95079-11-1
2-deoxy-2-(p-toluenesulfonamido)-α-D-mannopyranosyl 2-deoxy-2-(p-toluenesulfonamido)-α-D-mannopyranoside

: 95079-10-0
3,3'-dideoxy-3,3'-ditosylamino α-D-mannopyranosyl α-D-mannopyranoside 4,6,4',6'-tetraacetate

Guidance literature:: With osmium(VIII) oxide; sodium methylate; silver nitrate; Yield given. Multistep reaction. Yields of byproduct given; 1.) t-butyl alcohol/hexane, 40 deg C, 22 h, 2.) methanol, 15 min;
DOI:10.1016/0008-6215(84)85021-1