C₃₃H₄₂O₆

Base Information

Chemical Name:C₃₃H₄₂O₆
CAS No.:391278-02-7
Molecular Formula:C₃₃H₄₂O₆
Molecular Weight:534.693
Hs Code.:

C<sub>33</sub>H<sub>42</sub>O<sub>6</sub>

Synonyms:C₃₃H₄₂O₆

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Chemical Property of C₃₃H₄₂O₆

Chemical Property:

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Technology Process of C₃₃H₄₂O₆

There total 17 articles about C₃₃H₄₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 100-39-0
benzyl bromide

: 391278-01-6
C₁₉H₃₀O₆

: 391278-02-7
C₃₃H₄₂O₆

Guidance literature:: With sodium hydride; at 80 ℃;
DOI:10.1016/S0040-4039(01)01802-0

Reference yield:

: 2244-16-8,6485-40-1
(S)-p-mentha-6,8-dien-2-one

: 391278-02-7
C₃₃H₄₂O₆

Guidance literature:: Multi-step reaction with 11 steps

1.1: 92 percent / EtAlCl₂ / toluene; hexane / 28 h / 20 °C

2.1: 89 percent / p-TsOH / benzene / 12 h / Heating

3.1: N-methylmorpholine-N-oxide; OsO₄ / acetone; H₂O / 216 h / 20 °C

3.2: 74 percent / NaIO₄ / acetone; H₂O / 1 h / 20 °C

4.1: 93 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 72 h / 20 °C

5.1: 92 percent / p-TsOH / CH₂Cl₂ / 24 h / 20 °C

6.1: K₂CO₃ / methanol / 4 h / 20 °C

6.2: 90 percent / PCC / CH₂Cl₂ / 3 h / 20 °C

7.1: 88 percent / Et₃N / CH₂Cl₂ / 0.5 h / -78 °C

8.1: 73 percent / Na₂(EDTA); oxone; NaHCO₃ / H₂O; acetone; acetonitrile / 4 h / 20 °C

9.1: 79 percent / Al(OiPr)3 / toluene / 1 h / 20 °C

10.1: Me₃SiCl; Et₃N; DMAP / CH₂Cl₂ / 0.33 h / 20 °C

10.2: tetrahydrofuran / 0.17 h / -78 °C

10.3: 90 percent / HCl / tetrahydrofuran; H₂O / 0.5 h / 20 °C

11.1: NaH / tetrahydrofuran / 0 - 20 °C

11.2: 86 percent / tetrahydrofuran / 12 h / Heating

With dmap; Oxone; osmium(VIII) oxide; chloro-trimethyl-silane; ethylaluminum dichloride; edetate disodium; aluminum isopropoxide; sodium hydride; sodium hydrogencarbonate; potassium carbonate; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; hexane; dichloromethane; water; acetone; toluene; acetonitrile; benzene; 1.1: Diels-Alder reaction / 4.1: Baeyer-Villiger oxidation;
DOI:10.1016/j.tet.2004.07.094

Reference yield:

: 391278-09-4
6.8ac-Dimethyl-3c-isopropenyl-Δ⁶-(4arH)-octalon-(1)

: 391278-02-7
C₃₃H₄₂O₆

Guidance literature:: Multi-step reaction with 14 steps

1.1: 89 percent / H⁽¹⁺⁾

2.1: N-methylmorpholine-N-oxide / OsO₄

3.1: NaIO₄

4.1: 90 percent / m-chloroperbenzoic acid / CH₂Cl₂

5.1: 92 percent / H⁽¹⁺⁾

6.1: 100 percent / K₂CO₃ / methanol

7.1: 90 percent / pyridinium chlorochromate; 4 Angstroem MS / CH₂Cl₂

8.1: Et₃N

8.2: 89 percent / -78 °C

9.1: 73 percent / oxone / acetone

10.1: 79 percent / Al(Oi-Pr)3 / toluene

11.1: 96 percent / Et₃N

12.1: 100 percent / -78 °C

13.1: 90 percent / tetrabutylammonium fluoride / tetrahydrofuran

14.1: 86 percent / NaH / 80 °C

With Oxone; sodium periodate; 4 Angstroem MS; tetrabutyl ammonium fluoride; hydrogen cation; aluminum isopropoxide; sodium hydride; potassium carbonate; 4-methylmorpholine N-oxide; triethylamine; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; osmium(VIII) oxide; In tetrahydrofuran; methanol; dichloromethane; acetone; toluene; 4.1: Baeyer-Villiger oxidation / 10.1: Oppenauer ox. and Meerwein-Pondorf-Verley red.;
DOI:10.1016/S0040-4039(01)01802-0