1,2-bis(3,5-bis(tert-butyl)salicylaldimino)-4-(3-hydroxyphenoxy)benzene

Base Information

Chemical Name:1,2-bis(3,5-bis(tert-butyl)salicylaldimino)-4-(3-hydroxyphenoxy)benzene
CAS No.:1250266-77-3
Molecular Formula:C₄₂H₅₂N₂O₄
Molecular Weight:648.886
Hs Code.:

Synonyms:1,2-bis(3,5-bis(tert-butyl)salicylaldimino)-4-(3-hydroxyphenoxy)benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-bis(3,5-bis(tert-butyl)salicylaldimino)-4-(3-hydroxyphenoxy)benzene

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Technology Process of 1,2-bis(3,5-bis(tert-butyl)salicylaldimino)-4-(3-hydroxyphenoxy)benzene

There total 1 articles about 1,2-bis(3,5-bis(tert-butyl)salicylaldimino)-4-(3-hydroxyphenoxy)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 37942-07-7
3,5-di-tert-butyl-2-hydroxybenzaldehyde

: 43154-86-5
C₁₂H₁₂N₂O₂

: 1250266-77-3
1,2-bis(3,5-bis(tert-butyl)salicylaldimino)-4-(3-hydroxyphenoxy)benzene

Guidance literature:: In ethanol; at 80 ℃; Inert atmosphere;
DOI:10.1021/ja106484t

Reference yield: 90.0%

: 1250266-77-3
1,2-bis(3,5-bis(tert-butyl)salicylaldimino)-4-(3-hydroxyphenoxy)benzene

: 3375-31-3
palladium diacetate

: 1395342-72-9
C₄₂H₅₀N₂O₄Pd

Guidance literature:: In N,N-dimethyl-formamide; at 20 ℃; for 6h;
DOI:10.5560/ZNB.2012-0088

Reference yield: 71.0%

: 111-24-0
1,5-dibromo-pentane

: 1250266-77-3
1,2-bis(3,5-bis(tert-butyl)salicylaldimino)-4-(3-hydroxyphenoxy)benzene

: 1250266-81-9
(HO((CH₃)3C)2C₆H₂CHN)2C₆H₃OC₆H₄O(CH₂)5OC₆H₄OC₆H₃(NCHC₆H₂(C(CH₃)3)2OH)2

Guidance literature:: 1,2-bis(3,5-bis(tert-butyl)salicylaldimino)-4-(3-hydroxyphenoxy)benzene; With caesium carbonate; In acetonitrile; at 70 ℃; Inert atmosphere;

1,5-dibromo-pentane; With caesium carbonate; In acetonitrile; at 70 ℃; for 22h; Inert atmosphere;
DOI:10.1021/ja106484t