(2R,3S,4R)-1,3,4-tribenzyloxy-5-(4-methoxyphenyl)methylamino-6-hepten-2-ol

Base Information

Chemical Name:(2R,3S,4R)-1,3,4-tribenzyloxy-5-(4-methoxyphenyl)methylamino-6-hepten-2-ol
CAS No.:560130-10-1
Molecular Formula:C₃₆H₄₁NO₅
Molecular Weight:567.725
Hs Code.:

Synonyms:(2R,3S,4R)-1,3,4-tribenzyloxy-5-(4-methoxyphenyl)methylamino-6-hepten-2-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3S,4R)-1,3,4-tribenzyloxy-5-(4-methoxyphenyl)methylamino-6-hepten-2-ol

Chemical Property:

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Technology Process of (2R,3S,4R)-1,3,4-tribenzyloxy-5-(4-methoxyphenyl)methylamino-6-hepten-2-ol

There total 2 articles about (2R,3S,4R)-1,3,4-tribenzyloxy-5-(4-methoxyphenyl)methylamino-6-hepten-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1826-67-1
vinyl magnesium bromide

: 157831-24-8
((3S,4R,5R)-3,4-Bis-benzyloxy-5-benzyloxymethyl-tetrahydro-furan-2-yl)-(4-methoxy-benzyl)-amine

: 560130-10-1
(2R,3S,4R)-1,3,4-tribenzyloxy-5-(4-methoxyphenyl)methylamino-6-hepten-2-ol

Guidance literature:: In tetrahydrofuran; at 0 - 20 ℃; for 12.5h;
DOI:10.1016/S0040-4020(03)00378-8

Reference yield:

: 60933-68-8
3,4,6-tri-O-benzyl-β-D-arabinofuranoside

: 560130-10-1
(2R,3S,4R)-1,3,4-tribenzyloxy-5-(4-methoxyphenyl)methylamino-6-hepten-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 12 h / Heating

2: 23.7 g / tetrahydrofuran / 12.5 h / 0 - 20 °C

In tetrahydrofuran; toluene;
DOI:10.1016/S0040-4020(03)00378-8

Reference yield: 71.0%

: 560130-10-1
(2R,3S,4R)-1,3,4-tribenzyloxy-5-(4-methoxyphenyl)methylamino-6-hepten-2-ol

: 157831-26-0
(3S,4R,5S)-3,4-dibenzyloxy-1-(4-methoxyphenylmethyl)-5-vinylpyrrolidin-2-one

: (3S,4R,5R)-3,4-Bis-benzyloxy-1-(4-methoxy-benzyl)-5-vinyl-pyrrolidin-2-one

Guidance literature:: With 4 A molecular sieve; pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1016/S0040-4020(03)00378-8