10-(N-o-hydroxyphenylamide)-N-benzyl-7,7-dimethyl-dicyclo-<2,2,1>-heptane-2-imine

Base Information

Chemical Name:10-(N-o-hydroxyphenylamide)-N-benzyl-7,7-dimethyl-dicyclo-<2,2,1>-heptane-2-imine
CAS No.:127498-25-3
Molecular Formula:C₂₃H₂₆N₂O₂
Molecular Weight:362.472
Hs Code.:

Synonyms:10-(N-o-hydroxyphenylamide)-N-benzyl-7,7-dimethyl-dicyclo-<2,2,1>-heptane-2-imine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 10-(N-o-hydroxyphenylamide)-N-benzyl-7,7-dimethyl-dicyclo-<2,2,1>-heptane-2-imine

Chemical Property:

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Technology Process of 10-(N-o-hydroxyphenylamide)-N-benzyl-7,7-dimethyl-dicyclo-<2,2,1>-heptane-2-imine

There total 1 articles about 10-(N-o-hydroxyphenylamide)-N-benzyl-7,7-dimethyl-dicyclo-<2,2,1>-heptane-2-imine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 127498-24-2
(1S,4R)-7,7-Dimethyl-2-oxo-bicyclo[2.2.1]heptane-1-carboxylic acid (2-hydroxy-phenyl)-amide

: 100-46-9
benzylamine

: 127498-25-3
10-(N-o-hydroxyphenylamide)-N-benzyl-7,7-dimethyl-dicyclo-<2,2,1>-heptane-2-imine

Guidance literature:: In toluene;

Reference yield:

: 127498-25-3
10-(N-o-hydroxyphenylamide)-N-benzyl-7,7-dimethyl-dicyclo-<2,2,1>-heptane-2-imine

: 3886-69-9
(R)-1-phenyl-ethyl-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) butyllithium / 1.) hexane, THF, -78 deg C, 3 h

2: hydroxylamine acetate / 40 °C

With n-butyllithium; hydroxylamine acetate;

Reference yield:

: 127498-25-3
10-(N-o-hydroxyphenylamide)-N-benzyl-7,7-dimethyl-dicyclo-<2,2,1>-heptane-2-imine

: 2627-86-3
(S)-1-phenyl-ethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) butyllithium / 1.) hexane, THF, -78 deg C, 3 h

2: hydroxylamine acetate / 40 °C

With n-butyllithium; hydroxylamine acetate;