2,3-dihydro-2-(2-phenylethyl)-1H-naphtho[1,8-de]-1,3,2-diazaborine

Base Information

Chemical Name:2,3-dihydro-2-(2-phenylethyl)-1H-naphtho[1,8-de]-1,3,2-diazaborine
CAS No.:1245706-89-1
Molecular Formula:C₁₈H₁₇BN₂
Molecular Weight:272.157
Hs Code.:

Synonyms:2,3-dihydro-2-(2-phenylethyl)-1H-naphtho[1,8-de]-1,3,2-diazaborine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3-dihydro-2-(2-phenylethyl)-1H-naphtho[1,8-de]-1,3,2-diazaborine

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Technology Process of 2,3-dihydro-2-(2-phenylethyl)-1H-naphtho[1,8-de]-1,3,2-diazaborine

There total 10 articles about 2,3-dihydro-2-(2-phenylethyl)-1H-naphtho[1,8-de]-1,3,2-diazaborine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 2-(phenylethynyl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine

: 1245706-89-1
2,3-dihydro-2-(2-phenylethyl)-1H-naphtho[1,8-de]-1,3,2-diazaborine

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In 1,4-dioxane; at 20 ℃; for 1.33333h; Inert atmosphere; Schlenk technique;
DOI:10.1002/adsc.201400767

Reference yield: 95.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 1214264-88-6
2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine

: 1245706-89-1
2,3-dihydro-2-(2-phenylethyl)-1H-naphtho[1,8-de]-1,3,2-diazaborine

Guidance literature:: With [Cu(phen)(xantphosTEPD)]PF₆; potassium carbonate; In water; acetonitrile; at 20 ℃; for 7h; Sealed tube; Inert atmosphere; Irradiation;
DOI:10.1002/anie.202101874

Reference yield: 91.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 5656-71-3
2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine

: 1147458-75-0
2,3-dihydro-[B-2-(E)-1-phenylethen-1-yl]-1H-naphtho[1,8-de]-[1,3,2]-diazaborine

: 1245706-86-8
(C₁₀H₆)(NH)2BCH(CH₃)(C₆H₅)

: 1245706-89-1
2,3-dihydro-2-(2-phenylethyl)-1H-naphtho[1,8-de]-1,3,2-diazaborine

Guidance literature:: bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; In dioxane; mixt. of styrene, C10H9N2B and Rh complex in dioxane stirred at 60°C for 4 h under N2 atm.; sepd. by silica gel column chromy.;
DOI:10.1246/cl.2010.558