(Z)-4-(2-methoxybenzylidene)-2-(4-(trifluoromethyl)phenyl)oxazol-5(4H)-one

Base Information

Chemical Name:(Z)-4-(2-methoxybenzylidene)-2-(4-(trifluoromethyl)phenyl)oxazol-5(4H)-one
CAS No.:1402852-64-5
Molecular Formula:C₁₈H₁₂F₃NO₃
Molecular Weight:347.293
Hs Code.:

Synonyms:(Z)-4-(2-methoxybenzylidene)-2-(4-(trifluoromethyl)phenyl)oxazol-5(4H)-one

Suppliers and Price of (Z)-4-(2-methoxybenzylidene)-2-(4-(trifluoromethyl)phenyl)oxazol-5(4H)-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-4-(2-methoxybenzylidene)-2-(4-(trifluoromethyl)phenyl)oxazol-5(4H)-one

Chemical Property:

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Technology Process of (Z)-4-(2-methoxybenzylidene)-2-(4-(trifluoromethyl)phenyl)oxazol-5(4H)-one

There total 2 articles about (Z)-4-(2-methoxybenzylidene)-2-(4-(trifluoromethyl)phenyl)oxazol-5(4H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 25753-16-6
4-(trifluoromethyl)benzoic anhydride

: 1402852-64-5
(Z)-4-(2-methoxybenzylidene)-2-(4-(trifluoromethyl)phenyl)oxazol-5(4H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / dichloromethane / 0.33 h / Inert atmosphere; Reflux

2: sodium acetate / acetic anhydride / 2 h / Inert atmosphere; Reflux

With sodium acetate; sodium hydrogencarbonate; In dichloromethane; acetic anhydride;
DOI:10.1021/ja309003x DOI:10.1021/ja309003x

Reference yield:

: C₁₀H₆F₃NO₂

: 135-02-4
ortho-anisaldehyde

: 1402852-64-5
(Z)-4-(2-methoxybenzylidene)-2-(4-(trifluoromethyl)phenyl)oxazol-5(4H)-one

Guidance literature:: With sodium acetate; In acetic anhydride; for 2h; Inert atmosphere; Reflux;
DOI:10.1021/ja309003x DOI:10.1021/ja309003x

Reference yield: 64.0%

: 1402852-64-5
(Z)-4-(2-methoxybenzylidene)-2-(4-(trifluoromethyl)phenyl)oxazol-5(4H)-one

: 104883-33-2
malonic acid di(2,2,2-trifluoroethyl ester)

: 1402852-70-3
(5S,6R,9S)-bis(2,2,2-trifluoroethyl) 6-(2-methoxyphenyl)-4-oxo-2-(4-(trifluoromethyl)phenyl)-9-vinyl-3-oxa-1-azaspiro[4.4]non-1-ene-7,7-dicarboxylate

Guidance literature:: With trans-1,2-(1S,2S)-1,2-diaminocyclohexane-N,N’-bis(2’-diphenylphosphinobenzoyl); tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; In toluene; at 20 ℃; for 16.8333h; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja309003x DOI:10.1021/ja309003x