ethyl 3-(4-chlorophenyl)-3-oxo-2-((2,2,6,6-tetramethylpiperidin-1-yl)oxy)propanoate

Base Information

• Chemical Name: ethyl 3-(4-chlorophenyl)-3-oxo-2-((2,2,6,6-tetramethylpiperidin-1-yl)oxy)propanoate
• CAS No.: 1240506-03-9
• Molecular Formula: C₂₀H₂₈ClNO₄
• Molecular Weight: 381.9

Synonyms:ethyl 3-(4-chlorophenyl)-3-oxo-2-((2,2,6,6-tetramethylpiperidin-1-yl)oxy)propanoate

Chemical Property of ethyl 3-(4-chlorophenyl)-3-oxo-2-((2,2,6,6-tetramethylpiperidin-1-yl)oxy)propanoate

Chemical Property:

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Technology Process of ethyl 3-(4-chlorophenyl)-3-oxo-2-((2,2,6,6-tetramethylpiperidin-1-yl)oxy)propanoate

There total 2 articles about ethyl 3-(4-chlorophenyl)-3-oxo-2-((2,2,6,6-tetramethylpiperidin-1-yl)oxy)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

2,2,6,6-Tetramethyl-1-piperidinyloxy free radical (2564-83-2,45842-10-2,126517-51-9,25657-03-8,26933-82-4,54637-06-8,64104-42-3) + ethyl (4-chlorobenzoyl)acetate (2881-63-2) → ethyl 3-(4-chlorophenyl)-3-oxo-2-((2,2,6,6-tetramethylpiperidin-1-yl)oxy)propanoate (1240506-03-9)

Guidance literature:

With thieno[3,2-b]thiophene-2,5-dicarbaldehyde-4,4′,4′′,4′′′-(benzo[1,2-d:4,5-d′]bis(oxazole)-2,4,6,8-tetrayl)tetraaniline-integrated covalent organic frameworks; In acetonitrile; at 20 ℃; for 24h; Irradiation; Green chemistry;

DOI:10.1007/s11426-020-9931-4

Reference yield: 90.0%

→ ethyl 3-(4-chlorophenyl)-3-oxo-2-((2,2,6,6-tetramethylpiperidin-1-yl)oxy)propanoate (1240506-03-9)

Guidance literature:

With N₇₁₉ dye supported on titanium dioxide; In acetonitrile; for 48h; Irradiation; Green chemistry;

upstream raw materials:

2,2,6,6-Tetramethyl-1-piperidinyloxy free radical

ethyl (4-chlorobenzoyl)acetate

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