Carbamimidothioic acid, 2-(dimethylamino)-2-oxoethyl ester (9CI)

Base Information

Chemical Name:Carbamimidothioic acid, 2-(dimethylamino)-2-oxoethyl ester (9CI)
CAS No.:778549-46-5
Molecular Formula:C₅H₁₁N₃OS
Molecular Weight:161.228
Hs Code.:
Mol file:778549-46-5.mol

Synonyms:Carbamimidothioic acid, 2-(dimethylamino)-2-oxoethyl ester (9CI)

Suppliers and Price of Carbamimidothioic acid, 2-(dimethylamino)-2-oxoethyl ester (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of Carbamimidothioic acid, 2-(dimethylamino)-2-oxoethyl ester (9CI)

Chemical Property:

PSA：95.48000
LogP:0.50130

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Carbamimidothioic acid, 2-(dimethylamino)-2-oxoethyl ester (9CI)

There total 1 articles about Carbamimidothioic acid, 2-(dimethylamino)-2-oxoethyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 17356-08-0
thiourea

: 2675-89-0
2-chloro-N,N-dimethylacetamide

: 778549-46-5
2-carbamimidoylsulfanyl-N,N-dimethyl-acetamide

Guidance literature:: In acetone; at 20 ℃; for 16h;

Reference yield: 24.0%

: 778549-46-5
2-carbamimidoylsulfanyl-N,N-dimethyl-acetamide

: 540-72-7
sodium thiocyanide

: 881401-70-3
2-(5-Amino-[1,2,4]thiadiazol-3-ylsulfanyl)-N,N-dimethyl-acetamide

Guidance literature:: With bromine; sodium methylate; In methanol; at -15 ℃; for 1h;

Reference yield:

: 778549-46-5
2-carbamimidoylsulfanyl-N,N-dimethyl-acetamide

: 881401-57-6
(3-Dimethylcarbamoylmethylsulfanyl-[1,2,4]thiadiazol-5-yl)-(4-methoxy-benzyl)-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: bromine; sodium methylate / methanol / 1 h / -15 °C

2: dmap / tetrahydrofuran / 80 h / 20 - 60 °C

3: 1,8-diazabicyclo[5.4.0]undec-7-ene / 1,4-dioxane / 4 h / 80 °C

With dmap; bromine; sodium methylate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; 1,4-dioxane; methanol;