U(SePh)4(pyridine)3

Base Information

• Chemical Name: U(SePh)4(pyridine)3
• CAS No.: 910582-28-4
• Molecular Formula: C₃₉H₃₅N₃Se₄U
• Molecular Weight: 1099.6
• Mol file: 910582-28-4.mol

Synonyms:U(SePh)4(pyridine)3

Chemical Property of U(SePh)4(pyridine)3

Chemical Property:

Purity/Quality:

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Technology Process of U(SePh)4(pyridine)3

There total 1 articles about U(SePh)4(pyridine)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

pyridine (110-86-1) + uranium + diphenyl diselenide (1666-13-3) → U(SePh)4(pyridine)3 (910582-28-4)

Guidance literature:

iodine; In pyridine; under He; diphenyl diselenide and cat. amt. of I2 added to suspn. of U in pyridine, mixt. heated at 60°C for 36 h, stirred at ambient temp. for 6 d; filtered, filtrate evapd. under vac., viscous residue washed with hexanes, dried under vac., washed with hexanes, dried under vac.; elem. anal.;

DOI:10.1021/ic060560k

Reference yield:

U(SePh)4(pyridine)3 (910582-28-4) + acetonitrile (75-05-8,26809-02-9) → [U(SePh)2(μ2-SePh)2(acetonitrile)2]2

Guidance literature:

In acetonitrile; under He; U complex dissolved in CH3CN; crystn. by vapor diffusion of hexanes into soln.;

DOI:10.1021/ic060560k

upstream raw materials:

pyridine

diphenyl diselenide