N-methylmonoamide of threo-2,3-diphenylsuccinic acid

Base Information

Chemical Name:N-methylmonoamide of threo-2,3-diphenylsuccinic acid
CAS No.:136258-15-6
Molecular Formula:C₁₇H₁₇NO₃
Molecular Weight:283.327
Hs Code.:

Synonyms:N-methylmonoamide of threo-2,3-diphenylsuccinic acid

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Chemical Property of N-methylmonoamide of threo-2,3-diphenylsuccinic acid

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Technology Process of N-methylmonoamide of threo-2,3-diphenylsuccinic acid

There total 4 articles about N-methylmonoamide of threo-2,3-diphenylsuccinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 67311-05-1,67311-06-2,75693-05-9
trans-3,4-diphenyl-N-methylsuccinimide

: 136258-15-6
N-methylmonoamide of threo-2,3-diphenylsuccinic acid

Guidance literature:: With sodium hydroxide; In ethanol; water; for 0.25h; Heating;

Reference yield: 80.0%

: 858806-42-5
N,N'-dimethyldiamide of 2,3-diphenylsuccinic acid

: 136258-15-6
N-methylmonoamide of threo-2,3-diphenylsuccinic acid

Guidance literature:: With sodium hydroxide; In ethanol; water; for 4h; Heating;

Reference yield:

: 112363-47-0
N,N'-dimethyl-N,N'-di(phenylacetyl)hydrazine

: 136258-15-6
N-methylmonoamide of threo-2,3-diphenylsuccinic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) lithium hexamethyldisilazane, 2.) trimethylchlorosilane / 1.) THF, ether, HMPTA, -78 deg C, 30 min, 2.) THF, ether, HMPTA, reflux, 60 min

2: 75 percent / 90percent trifluoroacetic acid / 5 h / Heating

3: 90 percent / NaOH / ethanol; H₂O / 0.25 h / Heating

With sodium hydroxide; chloro-trimethyl-silane; trifluoroacetic acid; lithium hexamethyldisilazane; In ethanol; water;