(Z)-1-(benzothiazol-2-yl)-3-mercapto-3-(phenylamino)-2-(phenylsulfonyl)prop-2-en-1-one

Base Information

Chemical Name:(Z)-1-(benzothiazol-2-yl)-3-mercapto-3-(phenylamino)-2-(phenylsulfonyl)prop-2-en-1-one
CAS No.:1634722-92-1
Molecular Formula:C₂₂H₁₆N₂O₃S₃
Molecular Weight:452.579
Hs Code.:

Synonyms:(Z)-1-(benzothiazol-2-yl)-3-mercapto-3-(phenylamino)-2-(phenylsulfonyl)prop-2-en-1-one

Suppliers and Price of (Z)-1-(benzothiazol-2-yl)-3-mercapto-3-(phenylamino)-2-(phenylsulfonyl)prop-2-en-1-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-1-(benzothiazol-2-yl)-3-mercapto-3-(phenylamino)-2-(phenylsulfonyl)prop-2-en-1-one

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Technology Process of (Z)-1-(benzothiazol-2-yl)-3-mercapto-3-(phenylamino)-2-(phenylsulfonyl)prop-2-en-1-one

There total 1 articles about (Z)-1-(benzothiazol-2-yl)-3-mercapto-3-(phenylamino)-2-(phenylsulfonyl)prop-2-en-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1591907-98-0
1-(benzothiazol-2-yl)-2-phenylsulfonyl-1-ethanone

: 103-72-0
phenyl isothiocyanate

: 1634722-92-1
(Z)-1-(benzothiazol-2-yl)-3-mercapto-3-(phenylamino)-2-(phenylsulfonyl)prop-2-en-1-one

Guidance literature:: 1-(benzothiazol-2-yl)-2-phenylsulfonyl-1-ethanone; With potassium hydroxide; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

phenyl isothiocyanate; In N,N-dimethyl-formamide; at 20 ℃; for 6h;

With hydrogenchloride; In water; N,N-dimethyl-formamide; Cooling with ice;
DOI:10.3987/COM-14-13020

Reference yield: 94.0%

: 1634722-92-1
(Z)-1-(benzothiazol-2-yl)-3-mercapto-3-(phenylamino)-2-(phenylsulfonyl)prop-2-en-1-one

: 28663-68-5
ethyl (phenylhydrazono)chloroacetate

: 1634722-66-9
(Z)-ethyl 5-(2-(benzothiazol-2-yl)-2-oxo-1-(phenylsulfonyl)ethylidene)-4-phenyl-4,5-dihydro-1,3,4-thiadiazole-2-carboxylate

Guidance literature:: With triethylamine; In ethanol; at 150 ℃; for 0.333333h; under 12901.3 Torr; Microwave irradiation;
DOI:10.3987/COM-14-13020