(2S,4R,5R)-2,5-Bis(N,N-dibenzylamino)-4-O-(2,2,4,4-tetramethyl-1,3-oxazolidine-3-carbonyloxy)-3-heptanone

Base Information

Chemical Name:(2S,4R,5R)-2,5-Bis(N,N-dibenzylamino)-4-O-(2,2,4,4-tetramethyl-1,3-oxazolidine-3-carbonyloxy)-3-heptanone
CAS No.:247576-18-7
Molecular Formula:C₄₃H₅₃N₃O₄
Molecular Weight:675.912
Hs Code.:

Synonyms:(2S,4R,5R)-2,5-Bis(N,N-dibenzylamino)-4-O-(2,2,4,4-tetramethyl-1,3-oxazolidine-3-carbonyloxy)-3-heptanone

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Chemical Property of (2S,4R,5R)-2,5-Bis(N,N-dibenzylamino)-4-O-(2,2,4,4-tetramethyl-1,3-oxazolidine-3-carbonyloxy)-3-heptanone

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Technology Process of (2S,4R,5R)-2,5-Bis(N,N-dibenzylamino)-4-O-(2,2,4,4-tetramethyl-1,3-oxazolidine-3-carbonyloxy)-3-heptanone

There total 1 articles about (2S,4R,5R)-2,5-Bis(N,N-dibenzylamino)-4-O-(2,2,4,4-tetramethyl-1,3-oxazolidine-3-carbonyloxy)-3-heptanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 111060-49-2
N,N-dibenzyl-L-alanine benzyl ester

: 247576-09-6
2,2,4,4-Tetramethyl-oxazolidine-3-carboxylic acid (R)-2-dibenzylamino-butyl ester

: 247576-18-7
(2S,4R,5R)-2,5-Bis(N,N-dibenzylamino)-4-O-(2,2,4,4-tetramethyl-1,3-oxazolidine-3-carbonyloxy)-3-heptanone

Guidance literature:: 2,2,4,4-Tetramethyl-oxazolidine-3-carboxylic acid (R)-2-dibenzylamino-butyl ester; With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; In diethyl ether; hexane; cyclohexane; at -78 ℃; for 4h;

N,N-dibenzyl-L-alanine benzyl ester; In diethyl ether; hexane; cyclohexane; at -78 - 20 ℃; for 12h;
DOI:10.1055/s-1999-3576

Reference yield: 74.0%

: 247576-18-7
(2S,4R,5R)-2,5-Bis(N,N-dibenzylamino)-4-O-(2,2,4,4-tetramethyl-1,3-oxazolidine-3-carbonyloxy)-3-heptanone

: 247576-08-5
(2S,3R,4R,5R)-2,5-Bis(N,N-dibenzylamino)-4-O-(2,2,4,4-tetramethyl-1,3-oxazolidine-3-carbonyl)-3,4-heptanediol

: 247576-07-4
(2S,3S,4R,5R)-2,5-Bis(N,N-dibenzylamino)-4-O-(2,2,4,4-tetramethyl-1,3-oxazolidine-3-carbonyl)-3,4-heptanediol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 0 ℃; for 1h;
DOI:10.1055/s-1999-3576

Reference yield:

: 247576-18-7
(2S,4R,5R)-2,5-Bis(N,N-dibenzylamino)-4-O-(2,2,4,4-tetramethyl-1,3-oxazolidine-3-carbonyloxy)-3-heptanone

: (2S,3R,4R,5R)-2,5-Bis-dibenzylamino-heptane-3,4-diol

Guidance literature:: Multi-step reaction with 2 steps

1: 18 percent / LiAlH₄ / diethyl ether / 1 h / 0 °C

2: K₂CO₃ / methanol / 4 h / Heating

With lithium aluminium tetrahydride; potassium carbonate; In methanol; diethyl ether; 1: Reduction / 2: Hydrolysis;
DOI:10.1055/s-1999-3576