3'-(4-(4-chlorophenyl)-1H-imidazol-2-ylamino)-5'-(4-chlorophenyl)-4',5'-dihydropyrazole-1'-carbothioamide

Base Information

• Chemical Name: 3'-(4-(4-chlorophenyl)-1H-imidazol-2-ylamino)-5'-(4-chlorophenyl)-4',5'-dihydropyrazole-1'-carbothioamide
• CAS No.: 1616983-96-0
• Molecular Formula: C₁₉H₁₆Cl₂N₆S
• Molecular Weight: 431.348

Synonyms:3'-(4-(4-chlorophenyl)-1H-imidazol-2-ylamino)-5'-(4-chlorophenyl)-4',5'-dihydropyrazole-1'-carbothioamide

Chemical Property of 3'-(4-(4-chlorophenyl)-1H-imidazol-2-ylamino)-5'-(4-chlorophenyl)-4',5'-dihydropyrazole-1'-carbothioamide

Chemical Property:

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Technology Process of 3'-(4-(4-chlorophenyl)-1H-imidazol-2-ylamino)-5'-(4-chlorophenyl)-4',5'-dihydropyrazole-1'-carbothioamide

There total 3 articles about 3'-(4-(4-chlorophenyl)-1H-imidazol-2-ylamino)-5'-(4-chlorophenyl)-4',5'-dihydropyrazole-1'-carbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

C18H13Cl2N3O (1616983-87-9) + thiosemicarbazide (79-19-6) → 3'-(4-(4-chlorophenyl)-1H-imidazol-2-ylamino)-5'-(4-chlorophenyl)-4',5'-dihydropyrazole-1'-carbothioamide (1616983-96-0)

Guidance literature:

With sodium hydroxide; In ethanol; Reflux;

DOI:10.1016/j.ejmech.2014.06.001

Reference yield:

4-(4-chlorophenyl)-1H-imidazol-2-ylamine (60472-18-6) → 3'-(4-(4-chlorophenyl)-1H-imidazol-2-ylamino)-5'-(4-chlorophenyl)-4',5'-dihydropyrazole-1'-carbothioamide (1616983-96-0)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene

2: sodium hydroxide / ethanol / Reflux

With sodium hydroxide; In ethanol; toluene;

DOI:10.1016/j.ejmech.2014.06.001

Reference yield:

cinnamoyl chloride (35086-79-4,95602-71-4) → 3'-(4-(4-chlorophenyl)-1H-imidazol-2-ylamino)-5'-(4-chlorophenyl)-4',5'-dihydropyrazole-1'-carbothioamide (1616983-96-0)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene

2: sodium hydroxide / ethanol / Reflux

With sodium hydroxide; In ethanol; toluene;

DOI:10.1016/j.ejmech.2014.06.001

upstream raw materials:

C₁₈H₁₃Cl₂N₃O

thiosemicarbazide

4-(4-chlorophenyl)-1H-imidazol-2-ylamine

cinnamoyl chloride

Downstream raw materials:

3'-(4-(4-chlorophenyl)-1H-imidazol-2-ylamino)-5'-(4-chlorophenyl)-1'H-pyrazole-1'-carbothioamide

5'-(4-chlorophenyl)-N-(4-(4-chlorophenyl)-1H-imidazol-2-yl)-1'-(4-(4-chlorophenyl)thiazol-2-yl)-1'H-pyrazol-3'-amine

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