3-(4-methoxyphenyl)-N,N-dimethylpropiolamide

Base Information

Chemical Name:3-(4-methoxyphenyl)-N,N-dimethylpropiolamide
CAS No.:1051853-18-9
Molecular Formula:C₁₂H₁₃NO₂
Molecular Weight:203.241
Hs Code.:

Synonyms:3-(4-methoxyphenyl)-N,N-dimethylpropiolamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(4-methoxyphenyl)-N,N-dimethylpropiolamide

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Technology Process of 3-(4-methoxyphenyl)-N,N-dimethylpropiolamide

There total 8 articles about 3-(4-methoxyphenyl)-N,N-dimethylpropiolamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 768-60-5
4-methoxyphenylacetylen

: 79-44-7
N,N-Dimethylcarbamoyl chloride

: 1051853-18-9
3-(4-methoxyphenyl)-N,N-dimethylpropiolamide

Guidance literature:: 4-methoxyphenylacetylen; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.5h; Schlenk technique;

N,N-Dimethylcarbamoyl chloride; In tetrahydrofuran; at -78 - 20 ℃; Schlenk technique;
DOI:10.1039/c7cy02295f

Reference yield: 40.0%

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 768-60-5
4-methoxyphenylacetylen

: 1051853-18-9
3-(4-methoxyphenyl)-N,N-dimethylpropiolamide

Guidance literature:: With tert.-butylhydroperoxide; 2,6-bis(benzimidazole-2'-yl)pyridine; copper(II) choride dihydrate; lithium tert-butoxide; at 60 ℃; for 1h; Inert atmosphere;
DOI:10.1021/acscatal.5b02881

Reference yield: 39.0%

: 3-hydroxy-3-(4-methoxyphenyl)-N,N-dimethylpropanamide

: 1051853-18-9
3-(4-methoxyphenyl)-N,N-dimethylpropiolamide

Guidance literature:: With fluorosulfonyl fluoride; dimethyl sulfoxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; at 20 ℃; for 5h;
DOI:10.1021/jacs.8b10069