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Technology Process of {((p-tolyl)3P)12Au18Ag20Cl14}*42EtOH

{((p-tolyl)3P)12Au18Ag20Cl14}*42EtOH

Base Information
  • Chemical Name:{((p-tolyl)3P)12Au18Ag20Cl14}*42EtOH
  • CAS No.:129647-93-4
  • Molecular Formula:Ag20Au18*42C2H6O*12C21H21P*14Cl
  • Molecular Weight:11786.5
  • Hs Code.:
{((p-tolyl)3P)12Au<sub>18</sub>Ag<sub>20</sub>Cl<sub>14</sub>}*42EtOH

Synonyms:{((p-tolyl)3P)12Au18Ag20Cl14}*42EtOH

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Chemical Property of {((p-tolyl)3P)12Au18Ag20Cl14}*42EtOH
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Technology Process of {((p-tolyl)3P)12Au18Ag20Cl14}*42EtOH

There total 1 articles about {((p-tolyl)3P)12Au18Ag20Cl14}*42EtOH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

(tri-p-tolylphosphine)gold(I) chloride
28978-10-1

(tri-p-tolylphosphine)gold(I) chloride

((p-Tol)3PAgCl)4

((p-Tol)3PAgCl)4

{((p-tolyl)3P)12Au<sub>18</sub>Ag<sub>20</sub>Cl<sub>14</sub>}*42EtOH
129647-93-4

{((p-tolyl)3P)12Au18Ag20Cl14}*42EtOH

Guidance literature:
With NaBH4; NaSbF6; In ethanol; addn. of soln. of NaBH4 to mixt. of complexes in EtOH; reaction for 24 h; filtration; addn. of soln. of NaSbF6 to filtrate; stirred (few minutes); refiltration; recrystn. (ethanol/hexane 5/1) by evapn. under N2 at room temp.;
upstream raw materials:

(tri-p-tolylphosphine)gold(I) chloride

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