C₁₂H₁₂Cl₃NO₄

Base Information

• Chemical Name: C₁₂H₁₂Cl₃NO₄
• CAS No.: 1258181-30-4
• Molecular Formula: C₁₂H₁₂Cl₃NO₄
• Molecular Weight: 340.591
• Mol file: 1258181-30-4.mol

Synonyms:C₁₂H₁₂Cl₃NO₄

Chemical Property of C₁₂H₁₂Cl₃NO₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₂H₁₂Cl₃NO₄

There total 1 articles about C₁₂H₁₂Cl₃NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

acetyl chloride (75-36-5) + 2,2,2-trichloroethyl N-(p-methoxyphenyl)carbamate → C12H12Cl3NO4 (1258181-30-4)

Guidance literature:

With dmap; In acetonitrile; Reflux; Inert atmosphere;

DOI:10.1080/00397910903419910

Reference yield: 52.0%

C12H12Cl3NO4 (1258181-30-4) → 4-methoxyacetanilide (51-66-1)

Guidance literature:

C₁₂H₁₂Cl₃NO₄; With chloro-trimethyl-silane; mischmetal; In tetrahydrofuran; for 1.5h; Inert atmosphere; Reflux;

With water; In tetrahydrofuran; for 0.0833333h; Alkaline conditions;

DOI:10.1080/00397910903419910

upstream raw materials:

acetyl chloride

Downstream raw materials:

4-methoxyacetanilide