4,5-dimethoxy-2-(2,3,6,7-tetramethoxy-10-(pyren-1-yl)-anthracen-9-yl)benzoic acid

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Chemical Name:4,5-dimethoxy-2-(2,3,6,7-tetramethoxy-10-(pyren-1-yl)-anthracen-9-yl)benzoic acid
CAS No.:1414948-13-2
Molecular Formula:C₄₃H₃₄O₈
Molecular Weight:678.738
Hs Code.:

Synonyms:4,5-dimethoxy-2-(2,3,6,7-tetramethoxy-10-(pyren-1-yl)-anthracen-9-yl)benzoic acid

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Chemical Property of 4,5-dimethoxy-2-(2,3,6,7-tetramethoxy-10-(pyren-1-yl)-anthracen-9-yl)benzoic acid

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Technology Process of 4,5-dimethoxy-2-(2,3,6,7-tetramethoxy-10-(pyren-1-yl)-anthracen-9-yl)benzoic acid

There total 3 articles about 4,5-dimethoxy-2-(2,3,6,7-tetramethoxy-10-(pyren-1-yl)-anthracen-9-yl)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1414948-04-1
2-(10-bromo-2,3,6,7-tetramethoxyanthracen-9-yl)-4,5-dimethoxybenzoic acid

: 164461-18-1
1-pyrenylboronic acid

: 1414948-13-2
4,5-dimethoxy-2-(2,3,6,7-tetramethoxy-10-(pyren-1-yl)-anthracen-9-yl)benzoic acid

Guidance literature:: With potassium fluoride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; silver(l) oxide; In 2-methoxy-ethanol; at 130 ℃; for 48h; Sealed tube; Inert atmosphere;
DOI:10.1021/jo302139w

Reference yield:

: 1180-60-5
cyclotriveratrylene

: 1414948-13-2
4,5-dimethoxy-2-(2,3,6,7-tetramethoxy-10-(pyren-1-yl)-anthracen-9-yl)benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: potassium permanganate; manganese(IV) oxide; pyridine / 18 h / Reflux; Inert atmosphere

2: N-Bromosuccinimide; dibenzoyl peroxide / 1,2-dichloro-ethane / 2 h / 70 °C / Inert atmosphere

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium fluoride; silver(l) oxide / 2-methoxy-ethanol / 48 h / 130 °C / Sealed tube; Inert atmosphere

With pyridine; manganese(IV) oxide; potassium fluoride; potassium permanganate; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; silver(l) oxide; dibenzoyl peroxide; In 2-methoxy-ethanol; 1,2-dichloro-ethane; 3: |Suzuki Coupling;
DOI:10.1021/jo302139w

Reference yield:

: 127987-16-0
(2,3,7,8,12,13)-hexamethoxy-5H-tribenzo[a,d,g]cyclononene-5,10(15H)-dione

: 1414948-13-2
4,5-dimethoxy-2-(2,3,6,7-tetramethoxy-10-(pyren-1-yl)-anthracen-9-yl)benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide; dibenzoyl peroxide / 1,2-dichloro-ethane / 2 h / 70 °C / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium fluoride; silver(l) oxide / 2-methoxy-ethanol / 48 h / 130 °C / Sealed tube; Inert atmosphere

With potassium fluoride; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; silver(l) oxide; dibenzoyl peroxide; In 2-methoxy-ethanol; 1,2-dichloro-ethane; 2: |Suzuki Coupling;
DOI:10.1021/jo302139w