4-deacetyl-9,10-O-isopropylidene-2-(3-methoxybenzoyl)-1-deoxybaccatin VI

Base Information

Chemical Name:4-deacetyl-9,10-O-isopropylidene-2-(3-methoxybenzoyl)-1-deoxybaccatin VI
CAS No.:1451055-96-1
Molecular Formula:C₃₅H₄₆O₁₁
Molecular Weight:642.744
Hs Code.:

Synonyms:4-deacetyl-9,10-O-isopropylidene-2-(3-methoxybenzoyl)-1-deoxybaccatin VI

Suppliers and Price of 4-deacetyl-9,10-O-isopropylidene-2-(3-methoxybenzoyl)-1-deoxybaccatin VI

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-deacetyl-9,10-O-isopropylidene-2-(3-methoxybenzoyl)-1-deoxybaccatin VI

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-deacetyl-9,10-O-isopropylidene-2-(3-methoxybenzoyl)-1-deoxybaccatin VI

There total 5 articles about 4-deacetyl-9,10-O-isopropylidene-2-(3-methoxybenzoyl)-1-deoxybaccatin VI which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1451055-94-9
4,7,9,10-tetradeacetyl-2-desbenzoyl-2-m-methoxybenzoyl-9,10-O-isopropylidene-1-dehydroxybaccatin VI

: 108-24-7
acetic anhydride

: 1451055-96-1
4-deacetyl-9,10-O-isopropylidene-2-(3-methoxybenzoyl)-1-deoxybaccatin VI

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In toluene; for 5h; Heating;
DOI:10.1007/s00706-013-0981-z

Reference yield:

: 4,7,9,10,13-pentadeacetyl-1-dehydroxybaccatin VI

: 1451055-96-1
4-deacetyl-9,10-O-isopropylidene-2-(3-methoxybenzoyl)-1-deoxybaccatin VI

Guidance literature:: Multi-step reaction with 5 steps

1: Montmorillonite K₁₀ / 20 °C

2: N-benzyl-trimethylammonium hydroxide / 20 °C

3: dmap / tetrahydrofuran / 0 °C

4: dmap; dicyclohexyl-carbodiimide / toluene / 6 h / 50 °C

5: dmap; dicyclohexyl-carbodiimide / toluene / 5 h / Heating

With dmap; N-benzyl-trimethylammonium hydroxide; dicyclohexyl-carbodiimide; In tetrahydrofuran; toluene;
DOI:10.1007/s00706-013-0981-z

Reference yield:

: 939961-10-1
4,7,9,10,13-pentadeacetyl-9,10-O-isopropylidene-1-deoxybaccatin VI

: 1451055-96-1
4-deacetyl-9,10-O-isopropylidene-2-(3-methoxybenzoyl)-1-deoxybaccatin VI

Guidance literature:: Multi-step reaction with 4 steps

1: N-benzyl-trimethylammonium hydroxide / 20 °C

2: dmap / tetrahydrofuran / 0 °C

3: dmap; dicyclohexyl-carbodiimide / toluene / 6 h / 50 °C

4: dmap; dicyclohexyl-carbodiimide / toluene / 5 h / Heating

With dmap; N-benzyl-trimethylammonium hydroxide; dicyclohexyl-carbodiimide; In tetrahydrofuran; toluene;
DOI:10.1007/s00706-013-0981-z