10-acetyl-11-(2,4-dichlorophenyl)-3,3-dimethyl-1,1-dioxo-1,2,3,4,5,11-hexahydro-1λ6-thia-5,10-diazadibenzo[a,d]cycloheptene

Base Information

Chemical Name:10-acetyl-11-(2,4-dichlorophenyl)-3,3-dimethyl-1,1-dioxo-1,2,3,4,5,11-hexahydro-1λ6-thia-5,10-diazadibenzo[a,d]cycloheptene
CAS No.:1049088-65-4
Molecular Formula:C₂₂H₂₂Cl₂N₂O₃S
Molecular Weight:465.4
Hs Code.:

Synonyms:10-acetyl-11-(2,4-dichlorophenyl)-3,3-dimethyl-1,1-dioxo-1,2,3,4,5,11-hexahydro-1λ6-thia-5,10-diazadibenzo[a,d]cycloheptene

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Chemical Property of 10-acetyl-11-(2,4-dichlorophenyl)-3,3-dimethyl-1,1-dioxo-1,2,3,4,5,11-hexahydro-1λ6-thia-5,10-diazadibenzo[a,d]cycloheptene

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Technology Process of 10-acetyl-11-(2,4-dichlorophenyl)-3,3-dimethyl-1,1-dioxo-1,2,3,4,5,11-hexahydro-1λ6-thia-5,10-diazadibenzo[a,d]cycloheptene

There total 5 articles about 10-acetyl-11-(2,4-dichlorophenyl)-3,3-dimethyl-1,1-dioxo-1,2,3,4,5,11-hexahydro-1λ6-thia-5,10-diazadibenzo[a,d]cycloheptene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 1049093-46-0
C₂₀H₂₀Cl₂N₂O₂S

: 108-24-7
acetic anhydride

: 1049088-65-4
10-acetyl-11-(2,4-dichlorophenyl)-3,3-dimethyl-1,1-dioxo-1,2,3,4,5,11-hexahydro-1λ6-thia-5,10-diazadibenzo[a,d]cycloheptene

Guidance literature:: With toluene-4-sulfonic acid; at 70 ℃; for 6h;

Reference yield:

: 18615-62-8
5,5-dimethyl-dihydro-thiopyran-3-one

: 1049088-65-4
10-acetyl-11-(2,4-dichlorophenyl)-3,3-dimethyl-1,1-dioxo-1,2,3,4,5,11-hexahydro-1λ6-thia-5,10-diazadibenzo[a,d]cycloheptene

Guidance literature:: Multi-step reaction with 4 steps

1: 3-chloro-benzenecarboperoxoic acid / chloroform / 4 h

2: acetic acid / toluene / 15 h / 20 °C / Molecular sieve; Heating / reflux

3: toluene-4-sulfonic acid / dimethyl sulfoxide / 12 h / 75 °C

4: toluene-4-sulfonic acid / 6 h / 70 °C

With toluene-4-sulfonic acid; acetic acid; 3-chloro-benzenecarboperoxoic acid; In chloroform; dimethyl sulfoxide; toluene;

Reference yield:

: 1049093-44-8
C₇H₁₂O₂S

: 1049088-65-4
10-acetyl-11-(2,4-dichlorophenyl)-3,3-dimethyl-1,1-dioxo-1,2,3,4,5,11-hexahydro-1λ6-thia-5,10-diazadibenzo[a,d]cycloheptene

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / toluene / 15 h / 20 °C / Molecular sieve; Heating / reflux

2: toluene-4-sulfonic acid / dimethyl sulfoxide / 12 h / 75 °C

3: toluene-4-sulfonic acid / 6 h / 70 °C

With toluene-4-sulfonic acid; acetic acid; In dimethyl sulfoxide; toluene;