acrylic acid 2-[[3-butyrylamino-4-(4-cyano-3-methylisothiazol-5-ylazo)-phenyl]-(2-acryloyloxyethyl)-amino]-ethyl ester

Base Information

Chemical Name:acrylic acid 2-[[3-butyrylamino-4-(4-cyano-3-methylisothiazol-5-ylazo)-phenyl]-(2-acryloyloxyethyl)-amino]-ethyl ester
CAS No.:1357264-34-6
Molecular Formula:C₂₅H₂₈N₆O₅S
Molecular Weight:524.601
Hs Code.:

Synonyms:acrylic acid 2-[[3-butyrylamino-4-(4-cyano-3-methylisothiazol-5-ylazo)-phenyl]-(2-acryloyloxyethyl)-amino]-ethyl ester

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Chemical Property of acrylic acid 2-[[3-butyrylamino-4-(4-cyano-3-methylisothiazol-5-ylazo)-phenyl]-(2-acryloyloxyethyl)-amino]-ethyl ester

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Technology Process of acrylic acid 2-[[3-butyrylamino-4-(4-cyano-3-methylisothiazol-5-ylazo)-phenyl]-(2-acryloyloxyethyl)-amino]-ethyl ester

There total 4 articles about acrylic acid 2-[[3-butyrylamino-4-(4-cyano-3-methylisothiazol-5-ylazo)-phenyl]-(2-acryloyloxyethyl)-amino]-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1357264-33-5
N-[5-{bis-(2-hydroxyethyl)-amino}-2-(4-cyano-3-methylisothiazol-5-ylazo)-phenyl]-butyramide

: 625-36-5
2-chloropropionyl chloride

: 1357264-34-6
acrylic acid 2-[[3-butyrylamino-4-(4-cyano-3-methylisothiazol-5-ylazo)-phenyl]-(2-acryloyloxyethyl)-amino]-ethyl ester

Guidance literature:: With potassium carbonate; In tetrahydrofuran; at 50 ℃;

Reference yield:

: 1357264-31-3
N-[3-{bis-(2-hydroxyethyl)-amino}-phenyl]-butyramide

: 1357264-34-6
acrylic acid 2-[[3-butyrylamino-4-(4-cyano-3-methylisothiazol-5-ylazo)-phenyl]-(2-acryloyloxyethyl)-amino]-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid; propionic acid / 0.25 h / 20 °C

1.2: 0 - 5 °C

1.3: 0 - 20 °C

2.1: potassium carbonate / tetrahydrofuran / 50 °C

With potassium carbonate; acetic acid; propionic acid; In tetrahydrofuran;

Reference yield:

: N,N-bis-(2-hydroxyethyl)-m-phenylenediamine hydrochloride

: 1357264-34-6
acrylic acid 2-[[3-butyrylamino-4-(4-cyano-3-methylisothiazol-5-ylazo)-phenyl]-(2-acryloyloxyethyl)-amino]-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: calcium carbonate / water / 0.5 h / 20 °C

1.2: 1 h / 20 °C

2.1: acetic acid; propionic acid / 0.25 h / 20 °C

2.2: 0 - 5 °C

2.3: 0 - 20 °C

3.1: potassium carbonate / tetrahydrofuran / 50 °C

With potassium carbonate; acetic acid; propionic acid; calcium carbonate; In tetrahydrofuran; water;