3,5-Methanocyclopenta[b]pyrrole-1(2H)-carboxylicacid,hexahydro-,ethylester(9CI)

Base Information

Chemical Name:3,5-Methanocyclopenta[b]pyrrole-1(2H)-carboxylicacid,hexahydro-,ethylester(9CI)
CAS No.:78422-78-3
Molecular Formula:C₁₁H₁₇NO₂
Molecular Weight:195.261
Hs Code.:
Mol file:78422-78-3.mol

Synonyms:3,5-Methanocyclopenta[b]pyrrole-1(2H)-carboxylicacid,hexahydro-,ethylester(9CI)

Suppliers and Price of 3,5-Methanocyclopenta[b]pyrrole-1(2H)-carboxylicacid,hexahydro-,ethylester(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 3 raw suppliers

Chemical Property of 3,5-Methanocyclopenta[b]pyrrole-1(2H)-carboxylicacid,hexahydro-,ethylester(9CI)

Chemical Property:

PSA：29.54000
LogP:1.81110

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3,5-Methanocyclopenta[b]pyrrole-1(2H)-carboxylicacid,hexahydro-,ethylester(9CI)

There total 6 articles about 3,5-Methanocyclopenta[b]pyrrole-1(2H)-carboxylicacid,hexahydro-,ethylester(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.8%

: 541-41-3
chloroformic acid ethyl ester

: 55751-52-5
(1R,3R,6S,7R)-4-Methyl-4-aza-tricyclo[4.2.1.0^3,7]nonane

: 78422-78-3
(1S,3S,6R,7S)-4-Aza-tricyclo[4.2.1.0^3,7]nonane-4-carboxylic acid ethyl ester

Guidance literature:: In benzene; for 2h; Heating;
DOI:10.1016/S0040-4020(01)91182-2

Reference yield:

: 15907-62-7
2-((N-methylamino)methyl)bicyclo<2.2.1>hept-5-ene

: 78422-78-3
(1S,3S,6R,7S)-4-Aza-tricyclo[4.2.1.0^3,7]nonane-4-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / H₂ / PtO₂ / ethanol / 760 Torr

2: 2.08 g / NaOCl / CH₂Cl₂ / 1.75 h / Ambient temperature

3: 68 percent / trifluoroacetic acid / 2 h / Irradiation

4: 80.8 percent / benzene / 2 h / Heating

With sodium hypochlorite; hydrogen; platinum(IV) oxide; In ethanol; dichloromethane; trifluoroacetic acid; benzene;
DOI:10.1016/S0040-4020(01)91182-2

Reference yield:

: 39198-51-1
N-methyl-endo-bicyclo<2.2.1>hept-5-ene-2-carboxamide

: 78422-78-3
(1S,3S,6R,7S)-4-Aza-tricyclo[4.2.1.0^3,7]nonane-4-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 78 percent / LiAlH₄ / tetrahydrofuran / 13 h / Heating

2: 97 percent / H₂ / PtO₂ / ethanol / 760 Torr

3: 2.08 g / NaOCl / CH₂Cl₂ / 1.75 h / Ambient temperature

4: 68 percent / trifluoroacetic acid / 2 h / Irradiation

5: 80.8 percent / benzene / 2 h / Heating

With sodium hypochlorite; lithium aluminium tetrahydride; hydrogen; platinum(IV) oxide; In tetrahydrofuran; ethanol; dichloromethane; trifluoroacetic acid; benzene;
DOI:10.1016/S0040-4020(01)91182-2