(3R,5R)-5-dimethoxytrityloxy-1-N-tert-butyloxycarbonyl-3-hydroxypiperidine

Base Information

Chemical Name:(3R,5R)-5-dimethoxytrityloxy-1-N-tert-butyloxycarbonyl-3-hydroxypiperidine
CAS No.:1271240-67-5
Molecular Formula:C₃₁H₃₇NO₆
Molecular Weight:519.638
Hs Code.:

Synonyms:(3R,5R)-5-dimethoxytrityloxy-1-N-tert-butyloxycarbonyl-3-hydroxypiperidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3R,5R)-5-dimethoxytrityloxy-1-N-tert-butyloxycarbonyl-3-hydroxypiperidine

Chemical Property:

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Technology Process of (3R,5R)-5-dimethoxytrityloxy-1-N-tert-butyloxycarbonyl-3-hydroxypiperidine

There total 8 articles about (3R,5R)-5-dimethoxytrityloxy-1-N-tert-butyloxycarbonyl-3-hydroxypiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 1271240-62-0
(3R,5R)-1-N-tert-butyloxycarbonyl-3,5-dihydroxypiperidine

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 1271240-67-5
(3R,5R)-5-dimethoxytrityloxy-1-N-tert-butyloxycarbonyl-3-hydroxypiperidine

Guidance literature:: With pyridine; for 7h; Inert atmosphere;
DOI:10.1016/j.tet.2010.12.029

Reference yield:

: 1043449-04-2
(3R,5R)-dihydroxypiperidine

: 1271240-67-5
(3R,5R)-5-dimethoxytrityloxy-1-N-tert-butyloxycarbonyl-3-hydroxypiperidine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / ethanol; water / 2 h

2: pyridine / 7 h / Inert atmosphere

With pyridine; sodium hydrogencarbonate; In ethanol; water;
DOI:10.1016/j.tet.2010.12.029

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1271240-67-5
(3R,5R)-5-dimethoxytrityloxy-1-N-tert-butyloxycarbonyl-3-hydroxypiperidine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / ethanol; water / 2 h

2: pyridine / 7 h / Inert atmosphere

With pyridine; sodium hydrogencarbonate; In ethanol; water;
DOI:10.1016/j.tet.2010.12.029