N¹-(4-heptafluoroisopropyl-2-methylphenyl)-N²-[1-methyl-2-(methylthio)-ethyl]-3-methanesulfonyloxyphthalamide

Base Information

• Chemical Name: N¹-(4-heptafluoroisopropyl-2-methylphenyl)-N²-[1-methyl-2-(methylthio)-ethyl]-3-methanesulfonyloxyphthalamide
• CAS No.: 639513-21-6
• Molecular Formula: C₂₃H₂₃F₇N₂O₅S₂
• Molecular Weight: 604.567
• Mol file: 639513-21-6.mol

Synonyms:N¹-(4-heptafluoroisopropyl-2-methylphenyl)-N²-[1-methyl-2-(methylthio)-ethyl]-3-methanesulfonyloxyphthalamide

Chemical Property of N¹-(4-heptafluoroisopropyl-2-methylphenyl)-N²-[1-methyl-2-(methylthio)-ethyl]-3-methanesulfonyloxyphthalamide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of N¹-(4-heptafluoroisopropyl-2-methylphenyl)-N²-[1-methyl-2-(methylthio)-ethyl]-3-methanesulfonyloxyphthalamide

There total 1 articles about N¹-(4-heptafluoroisopropyl-2-methylphenyl)-N²-[1-methyl-2-(methylthio)-ethyl]-3-methanesulfonyloxyphthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methyl-4-(heptafluoropropan-2-yl)-aniline (238098-26-5) + 3-hydroxyphthalic anhydride (37418-88-5) + 1-methyl-2-(methylthio)ethylamine (13296-25-8) + methanesulfonyl chloride (124-63-0) + methyl chloroformate (79-22-1) → N1-(4-heptafluoroisopropyl-2-methylphenyl)-N2-[1-methyl-2-(methylthio)-ethyl]-3-methanesulfonyloxyphthalamide (639513-21-6)

Guidance literature:

3-hydroxyphthalic anhydride; methanesulfonyl chloride; With triethylamine; In 1,2-dichloro-ethane; at 50 ℃; for 1.5h;

1-methyl-2-(methylthio)ethylamine; With triethylamine; In 1,2-dichloro-ethane; at 20 ℃; for 2h;

2-methyl-4-(heptafluoropropan-2-yl)-aniline; methyl chloroformate; With hydrogenchloride; sodium hydrogencarbonate; more than 3 stages;

upstream raw materials:

2-methyl-4-(heptafluoropropan-2-yl)-aniline

3-hydroxyphthalic anhydride

1-methyl-2-(methylthio)ethylamine

methanesulfonyl chloride

Refernces