Technology Process of C53H59NO4Si
There total 4 articles about C53H59NO4Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere
2: sodium iodide / acetone / 18 h / Darkness; Reflux; Inert atmosphere
3: lithium chloride; lithium diisopropyl amide / tetrahydrofuran
With
triethylamine; sodium iodide; lithium chloride; lithium diisopropyl amide;
In
tetrahydrofuran; acetone;
3: |Myers's Alkylation;
DOI:10.3762/bjoc.9.132
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium iodide / acetone / 18 h / Darkness; Reflux; Inert atmosphere
2: lithium chloride; lithium diisopropyl amide / tetrahydrofuran
With
sodium iodide; lithium chloride; lithium diisopropyl amide;
In
tetrahydrofuran; acetone;
2: |Myers's Alkylation;
DOI:10.3762/bjoc.9.132
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium; lithium chloride / tetrahydrofuran; hexane / 0.5 h / 0 °C / Inert atmosphere
1.2: 3 h / 0 - 20 °C / Inert atmosphere
2.1: dmap; triethylamine / dichloromethane
3.1: lithium chloride; lithium diisopropyl amide / tetrahydrofuran
With
dmap; n-butyllithium; triethylamine; lithium chloride; lithium diisopropyl amide;
In
tetrahydrofuran; hexane; dichloromethane;
3.1: |Myers's Alkylation;
DOI:10.3762/bjoc.9.132
