9H-Pyrido[3,4-b]indole-3-carboxaldehyde,1-methyl-(9CI)

Base Information

Chemical Name:9H-Pyrido[3,4-b]indole-3-carboxaldehyde,1-methyl-(9CI)
CAS No.:777062-70-1
Molecular Formula:C13H10 N2 O
Molecular Weight:210.2313
Hs Code.:
Mol file:777062-70-1.mol

Synonyms:9H-Pyrido[3,4-b]indole-3-carboxaldehyde,1-methyl-(9CI)

Suppliers and Price of 9H-Pyrido[3,4-b]indole-3-carboxaldehyde,1-methyl-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AccelPharmtech
1-methyl-9H-Pyrido[3,4-b]indole-3-carboxaldehyde 97.00%
5G
$ 4530.00

AccelPharmtech
1-methyl-9H-Pyrido[3,4-b]indole-3-carboxaldehyde 97.00%
1G
$ 2640.00

Total 1 raw suppliers

Chemical Property of 9H-Pyrido[3,4-b]indole-3-carboxaldehyde,1-methyl-(9CI)

Chemical Property:

PSA：45.75000
LogP:2.83700

Purity/Quality:: 1-methyl-9H-Pyrido[3,4-b]indole-3-carboxaldehyde 97.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 9H-Pyrido[3,4-b]indole-3-carboxaldehyde,1-methyl-(9CI)

There total 10 articles about 9H-Pyrido[3,4-b]indole-3-carboxaldehyde,1-methyl-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 33821-72-6
(1-methyl-9H-pyrido[3,4-b]indol-3-yl)methanol

: 777062-70-1
1-methyl-9H-pyrido[3,4-b]indole-3-carbaldehyde

Guidance literature:: With manganese(IV) oxide; In dichloromethane; for 48h; Heating;
DOI:10.1002/jhet.5570410409

Reference yield:

: 33821-71-5
ethyl 1-methyl-9H-pyrido[3,4-b]indole-3-carboxylateyl-2,3,4,9-tetrahydro-1Hpyrido[3,4-b]indole-3-carboxylate

: 777062-70-1
1-methyl-9H-pyrido[3,4-b]indole-3-carbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

2: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 20 °C

With lithium aluminium tetrahydride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1021/jf404840x

Reference yield:

: 73-22-3,27732-43-0,80206-30-0,27813-82-7
L-Tryptophan

: 777062-70-1
1-methyl-9H-pyrido[3,4-b]indole-3-carbaldehyde

Guidance literature:: Multi-step reaction with 5 steps

1: sulfuric acid / water / 20 °C

2: thionyl chloride / water / 5 h / Reflux

3: sulfur / 5,5-dimethyl-1,3-cyclohexadiene / 12 h / Reflux

4: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

5: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 20 °C

With lithium aluminium tetrahydride; thionyl chloride; sulfuric acid; sulfur; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; water; dimethyl sulfoxide; 1: |Pictet-Spengler Synthesis;
DOI:10.1021/jf404840x