2-(trimethylsilylethynyl)trifluoroacetanilide

Base Information

Chemical Name:2-(trimethylsilylethynyl)trifluoroacetanilide
CAS No.:316795-01-4
Molecular Formula:C₁₃H₁₄F₃NOSi
Molecular Weight:285.341
Hs Code.:

Synonyms:2-(trimethylsilylethynyl)trifluoroacetanilide

Suppliers and Price of 2-(trimethylsilylethynyl)trifluoroacetanilide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(trimethylsilylethynyl)trifluoroacetanilide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-(trimethylsilylethynyl)trifluoroacetanilide

There total 4 articles about 2-(trimethylsilylethynyl)trifluoroacetanilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 103529-16-4
2-[(trimethylsilyl)ethynyl]aniline

: 407-25-0
trifluoroacetic anhydride

: 316795-01-4
2-(trimethylsilylethynyl)trifluoroacetanilide

Guidance literature:: With dmap; In dichloromethane; at 20 ℃; for 15h;

Reference yield: 99.0%

: 143321-89-5
2,2,2-trifluoro-N-(2-iodophenyl)acetamide

: 1066-54-2
trimethylsilylacetylene

: 316795-01-4
2-(trimethylsilylethynyl)trifluoroacetanilide

Guidance literature:: With copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; at 20 ℃; for 24h;
DOI:10.1021/ol049762f

Reference yield:

: 615-43-0
2-iodophenylamine

: 316795-01-4
2-(trimethylsilylethynyl)trifluoroacetanilide

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / Et₃N / tetrahydrofuran / -15 - 25 °C

2: 99 percent / Et₃N; CuI / PdCl₂(PPh₃)2 / tetrahydrofuran / 24 h / 20 °C

With copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran;
DOI:10.1021/ol049762f