N'-(1-benzylpiperidin-4-ylidene)-2,4,6-triisopropylbenzenesulfonohydrazide

Base Information

Chemical Name:N'-(1-benzylpiperidin-4-ylidene)-2,4,6-triisopropylbenzenesulfonohydrazide
CAS No.:1448295-64-4
Molecular Formula:C₂₇H₃₉N₃O₂S
Molecular Weight:469.692
Hs Code.:

Synonyms:N'-(1-benzylpiperidin-4-ylidene)-2,4,6-triisopropylbenzenesulfonohydrazide

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Chemical Property of N'-(1-benzylpiperidin-4-ylidene)-2,4,6-triisopropylbenzenesulfonohydrazide

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Technology Process of N'-(1-benzylpiperidin-4-ylidene)-2,4,6-triisopropylbenzenesulfonohydrazide

There total 2 articles about N'-(1-benzylpiperidin-4-ylidene)-2,4,6-triisopropylbenzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 3612-20-2
1-phenylmethyl-4-piperidone

: 39085-59-1
trisylhydrazine

: 1448295-64-4
N'-(1-benzylpiperidin-4-ylidene)-2,4,6-triisopropylbenzenesulfonohydrazide

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; at 20 ℃; for 3.5h; Inert atmosphere;
DOI:10.1021/ol401637n

Reference yield:

: 6553-96-4
2,4,6-triisopropylphenylsulfonyl chloride

: 1448295-64-4
N'-(1-benzylpiperidin-4-ylidene)-2,4,6-triisopropylbenzenesulfonohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine / tetrahydrofuran / 3 h / -10 - 0 °C

2: hydrogenchloride / tetrahydrofuran / 3.5 h / 20 °C / Inert atmosphere

With hydrogenchloride; hydrazine; In tetrahydrofuran;
DOI:10.1021/ol401637n

Reference yield: 23.0%

: 1448295-64-4
N'-(1-benzylpiperidin-4-ylidene)-2,4,6-triisopropylbenzenesulfonohydrazide

: 1448295-70-2
1-benzyl-4-fluoro-1,2,3,6-tetrahydropyridine

Guidance literature:: N'-(1-benzylpiperidin-4-ylidene)-2,4,6-triisopropylbenzenesulfonohydrazide; With n-butyllithium; In tetrahydrofuran; at -78 - 0 ℃; for 0.833333h;

With 1-fluoro-1,1-bis(phenylsulfonyl)methane; In tetrahydrofuran; at -78 - 20 ℃; for 2.5h;
DOI:10.1021/ol401637n