N-acetyl-2,3,4-tri-O-benzyl-N-(benzyl N-benzyloxycarbonyl-L-β-aspartyl)-6-O-tert-butyldiphenylsilyl-α-D-glucopyranosylamine

Base Information

• Chemical Name: N-acetyl-2,3,4-tri-O-benzyl-N-(benzyl N-benzyloxycarbonyl-L-β-aspartyl)-6-O-tert-butyldiphenylsilyl-α-D-glucopyranosylamine
• CAS No.: 127570-64-3
• Molecular Formula: C₆₄H₆₈N₂O₁₁Si
• Molecular Weight: 1069.34

Synonyms:N-acetyl-2,3,4-tri-O-benzyl-N-(benzyl N-benzyloxycarbonyl-L-β-aspartyl)-6-O-tert-butyldiphenylsilyl-α-D-glucopyranosylamine

Chemical Property of N-acetyl-2,3,4-tri-O-benzyl-N-(benzyl N-benzyloxycarbonyl-L-β-aspartyl)-6-O-tert-butyldiphenylsilyl-α-D-glucopyranosylamine

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of N-acetyl-2,3,4-tri-O-benzyl-N-(benzyl N-benzyloxycarbonyl-L-β-aspartyl)-6-O-tert-butyldiphenylsilyl-α-D-glucopyranosylamine

There total 11 articles about N-acetyl-2,3,4-tri-O-benzyl-N-(benzyl N-benzyloxycarbonyl-L-β-aspartyl)-6-O-tert-butyldiphenylsilyl-α-D-glucopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

Z-Asp-OBn (4779-31-1) + phenyl 2,3,4-tri-O-benzyl-6-O-tert-butyldiphenylsilyl-1-thio-β-D-glucopyranoside (139299-89-1) + acetonitrile (75-05-8,26809-02-9) → N-acetyl-2,3,4-tri-O-benzyl-N-(benzyl N-benzyloxycarbonyl-L-β-aspartyl)-6-O-tert-butyldiphenylsilyl-α-D-glucopyranosylamine (127570-64-3)

Guidance literature:

With N-iodo-succinimide; In acetonitrile; Ambient temperature;

DOI:10.1016/0040-4039(91)80430-E

Reference yield: 61.0%

Z-Asp-OBn (4779-31-1) + tert-Butyl-diphenyl-{(2R,3R,4S,5R)-3,4,5-tris-benzyloxy-6-[((E)-pent-1-enyl)oxy]-tetrahydro-pyran-2-ylmethoxy}-silane + acetonitrile (75-05-8,26809-02-9) → N-acetyl-2,3,4-tri-O-benzyl-N-(benzyl N-benzyloxycarbonyl-L-β-aspartyl)-6-O-tert-butyldiphenylsilyl-α-D-glucopyranosylamine (127570-64-3)

Guidance literature:

With N-Bromosuccinimide;

DOI:10.1021/ja00170a055

Reference yield: 61.0%

Z-Asp-OBn (4779-31-1) + pent-4-enyl 2,3,4-tri-O-benzyl-6-O-tert-butyldiphenylsilyl-D-glucopyranoside (441310-81-2) + acetonitrile (75-05-8,26809-02-9) → N-acetyl-2,3,4-tri-O-benzyl-N-(benzyl N-benzyloxycarbonyl-L-β-aspartyl)-6-O-tert-butyldiphenylsilyl-α-D-glucopyranosylamine (127570-64-3)

Guidance literature:

With N-Bromosuccinimide; for 1h; Ambient temperature;

DOI:10.1016/0008-6215(92)84171-N

upstream raw materials:

Z-Asp-OBn

acetonitrile

phenyl 2,3,4-tri-O-benzyl-6-O-tert-butyldiphenylsilyl-1-thio-β-D-glucopyranoside

pent-4-enyl 2,3,4-tri-O-benzyl-6-O-tert-butyldiphenylsilyl-D-glucopyranoside

Downstream raw materials:

2,3,4-tri-O-benzyl-N-(benzyl N-benzyloxycarbonyl-L-β-aspartyl)-6-O-tert-butyldiphenylsilyl-α-D-glucopyranosylamine

2,3,4-tri-O-benzyl-N-(benzyl N-benzyloxycarbonyl-L-β-aspartyl)-α-D-glucopyranosylamine

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