3-amino-N-{3-[(2-chloro-5-methoxyphenyl)amino]quinoxalin-2-yl}benzenesulfonamide hydrochloride

Base Information

Chemical Name:3-amino-N-{3-[(2-chloro-5-methoxyphenyl)amino]quinoxalin-2-yl}benzenesulfonamide hydrochloride
CAS No.:1433222-74-2
Molecular Formula:C₂₁H₁₈ClN₅O₃S*ClH
Molecular Weight:492.386
Hs Code.:

Synonyms:3-amino-N-{3-[(2-chloro-5-methoxyphenyl)amino]quinoxalin-2-yl}benzenesulfonamide hydrochloride

Suppliers and Price of 3-amino-N-{3-[(2-chloro-5-methoxyphenyl)amino]quinoxalin-2-yl}benzenesulfonamide hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-amino-N-{3-[(2-chloro-5-methoxyphenyl)amino]quinoxalin-2-yl}benzenesulfonamide hydrochloride

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of 3-amino-N-{3-[(2-chloro-5-methoxyphenyl)amino]quinoxalin-2-yl}benzenesulfonamide hydrochloride

There total 4 articles about 3-amino-N-{3-[(2-chloro-5-methoxyphenyl)amino]quinoxalin-2-yl}benzenesulfonamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 934528-15-1
N-(3-((2-chloro-5-methoxyphenyl)amino)quinoxalin-2-yl)-3-nitrobenzenesulfonamide

: 1433222-74-2
3-amino-N-{3-[(2-chloro-5-methoxyphenyl)amino]quinoxalin-2-yl}benzenesulfonamide hydrochloride

Guidance literature:: N-(3-((2-chloro-5-methoxyphenyl)amino)quinoxalin-2-yl)-3-nitrobenzenesulfonamide; With potassium formate; In tetrahydrofuran; ethanol; water; Reflux; Large scale;

With hydrogenchloride; In tetrahydrofuran; methanol; ethanol; water; at 20 ℃; Large scale;

Reference yield:

: 2213-63-0
2,3-dichloroquinoxaline

: 1433222-74-2
3-amino-N-{3-[(2-chloro-5-methoxyphenyl)amino]quinoxalin-2-yl}benzenesulfonamide hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / Reflux; Industrial scale

2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / Reflux; Industrial scale

3.1: potassium formate; platinum sulfide on carbon / tetrahydrofuran; water; ethanol / Reflux; Industrial scale

3.2: 20 °C / Industrial scale

With platinum sulfide on carbon; potassium formate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; ethanol; water; acetonitrile;

Reference yield:

: 121-52-8
3-nitrophenylsulfonamide

: 1433222-74-2
3-amino-N-{3-[(2-chloro-5-methoxyphenyl)amino]quinoxalin-2-yl}benzenesulfonamide hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / Reflux; Industrial scale

2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / Reflux; Industrial scale

3.1: potassium formate; platinum sulfide on carbon / tetrahydrofuran; water; ethanol / Reflux; Industrial scale

3.2: 20 °C / Industrial scale

With platinum sulfide on carbon; potassium formate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; ethanol; water; acetonitrile;