C₂₄H₂₉NO₄

Base Information

Chemical Name:C₂₄H₂₉NO₄
CAS No.:251651-05-5
Molecular Formula:C₂₄H₂₉NO₄
Molecular Weight:395.499
Hs Code.:

C<sub>24</sub>H<sub>29</sub>NO<sub>4</sub>

Synonyms:C₂₄H₂₉NO₄

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Chemical Property of C₂₄H₂₉NO₄

Chemical Property:

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Technology Process of C₂₄H₂₉NO₄

There total 18 articles about C₂₄H₂₉NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (R)-2-[(E)-3-(Dimethyl-phenyl-silanyl)-allyl]-5-methyl-cyclohex-2-enone

: 251651-05-5
C₂₄H₂₉NO₄

Guidance literature:: Multi-step reaction with 18 steps

1.1: CuI

2.1: NaI; mCPBA

3.1: 82 percent / Bu₃SnH; AIBN / benzene / Heating

4.1: Li; NH₃

5.1: TBAF

5.2: KHCO₃; H₂O₂ / methanol

6.1: 95 percent / imidazole

7.1: 90 percent / PCC

8.1: 88 percent / L-Selectride

9.1: 87 percent / KH / tetrahydrofuran

10.1: 82 percent / CF₃COOH

11.1: SeO₂ / dioxane

13.1: LiClO₄ / diethyl ether / 20 °C

14.1: aq. AcOH / tetrahydrofuran

15.1: 86 percent

16.1: (COCl)2

18.1: K₂CO₃ / xylene / Heating

With 1H-imidazole; copper(l) iodide; selenium(IV) oxide; oxalyl dichloride; 2,2'-azobis(isobutyronitrile); tetrabutyl ammonium fluoride; ammonia; tri-n-butyl-tin hydride; lithium perchlorate; lithium; potassium hydride; L-Selectride; potassium carbonate; acetic acid; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; trifluoroacetic acid; sodium iodide; In tetrahydrofuran; 1,4-dioxane; diethyl ether; xylene; benzene; 1.1: addition; silylation / 2.1: Iodination / 3.1: Cyclization / 4.1: Reduction / 5.1: Substitution / 5.2: Oxidation / 6.1: silylation / 7.1: Oxidation / 8.1: Reduction / 9.1: benzylation / 10.1: desilylation / 11.1: allylic oxidation / 12.1: Swern oxidation / 13.1: Addition / 14.1: desilylation / 15.1: Jones oxidation / 16.1: Chlorination / 17.1: Substitution / 18.1: Cyclization;
DOI:10.1021/ja992315o

Reference yield:

: 251650-95-0
(2S,5aR,7R,9R,9aS)-2-Hydroxymethyl-7-methyl-3-trimethylsilanyl-2,4,5,5a,6,7,8,9-octahydro-1H-cyclopenta[c]inden-9-ol

: 251651-05-5
C₂₄H₂₉NO₄

Guidance literature:: Multi-step reaction with 13 steps

1: 95 percent / imidazole

2: 90 percent / PCC

3: 88 percent / L-Selectride

4: 87 percent / KH / tetrahydrofuran

5: 82 percent / CF₃COOH

6: SeO₂ / dioxane

8: LiClO₄ / diethyl ether / 20 °C

9: aq. AcOH / tetrahydrofuran

10: 86 percent

11: (COCl)2

13: K₂CO₃ / xylene / Heating

With 1H-imidazole; selenium(IV) oxide; oxalyl dichloride; lithium perchlorate; potassium hydride; L-Selectride; potassium carbonate; acetic acid; pyridinium chlorochromate; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; diethyl ether; xylene; 1: silylation / 2: Oxidation / 3: Reduction / 4: benzylation / 5: desilylation / 6: allylic oxidation / 7: Swern oxidation / 8: Addition / 9: desilylation / 10: Jones oxidation / 11: Chlorination / 12: Substitution / 13: Cyclization;
DOI:10.1021/ja992315o

Reference yield:

: 251650-99-4
(9-benzyloxy-7-methyl-2,4,5,5a,6,7,8,9-octahydro-1H-cyclopenta[c]inden-2-ylmethoxy)-tert-butyl-dimethyl-silane

: 251651-05-5
C₂₄H₂₉NO₄

Guidance literature:: Multi-step reaction with 8 steps

1: SeO₂ / dioxane

3: LiClO₄ / diethyl ether / 20 °C

4: aq. AcOH / tetrahydrofuran

5: 86 percent

6: (COCl)2

8: K₂CO₃ / xylene / Heating

With selenium(IV) oxide; oxalyl dichloride; lithium perchlorate; potassium carbonate; acetic acid; In tetrahydrofuran; 1,4-dioxane; diethyl ether; xylene; 1: allylic oxidation / 2: Swern oxidation / 3: Addition / 4: desilylation / 5: Jones oxidation / 6: Chlorination / 7: Substitution / 8: Cyclization;
DOI:10.1021/ja992315o