1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-methylidenehydrazine

Base Information

Chemical Name:1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-methylidenehydrazine
CAS No.:1363809-36-2
Molecular Formula:C₁₅H₂₀N₂O₂
Molecular Weight:260.336
Hs Code.:

Synonyms:1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-methylidenehydrazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-methylidenehydrazine

Chemical Property:

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Technology Process of 1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-methylidenehydrazine

There total 10 articles about 1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-methylidenehydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1363807-14-0
1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methylhydrazine

: 1363809-36-2
1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-methylidenehydrazine

Guidance literature:: In methanol; water; at 20 ℃; for 2.5h;

Reference yield:

: 314084-61-2
1-bromo-2,6-diethyl-4-methylbenzene

: 1363809-36-2
1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-methylidenehydrazine

Guidance literature:: Multi-step reaction with 6 steps

1.1: magnesium; ethylene dibromide / toluene; tetrahydrofuran / 52 h / 40 - 50 °C / Inert atmosphere

1.2: 2 h / 0 - 5 °C / Inert atmosphere

2.1: hydrazine hydrate / methanol / 4.08 h / 1 - 2 °C

3.1: methanol / 1.5 h / 20 °C

4.1: potassium carbonate / N,N-dimethyl-formamide / 2.5 h / 20 °C

5.1: hydroxylamine / water; methanol / 17 h / 50 - 60 °C

6.1: water; methanol / 2.5 h / 20 °C

With hydroxylamine; potassium carbonate; hydrazine hydrate; magnesium; ethylene dibromide; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1363806-98-7
ethyl 2-(2,6-diethyl-4-methylphenyl)-2-oxoacetate

: 1363809-36-2
1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-methylidenehydrazine

Guidance literature:: Multi-step reaction with 5 steps

1: hydrazine hydrate / methanol / 4.08 h / 1 - 2 °C

2: methanol / 1.5 h / 20 °C

3: potassium carbonate / N,N-dimethyl-formamide / 2.5 h / 20 °C

4: hydroxylamine / water; methanol / 17 h / 50 - 60 °C

5: water; methanol / 2.5 h / 20 °C

With hydroxylamine; potassium carbonate; hydrazine hydrate; In methanol; water; N,N-dimethyl-formamide;