methoxy(5-(4-(N,N-dimethylamino)phenyl)ethynyl-10,15-diphenylsubporphyrinato)boron(III)

Base Information

Chemical Name:methoxy(5-(4-(N,N-dimethylamino)phenyl)ethynyl-10,15-diphenylsubporphyrinato)boron(III)
CAS No.:1392132-11-4
Molecular Formula:C₃₈H₂₉BN₄O
Molecular Weight:568.485
Hs Code.:

Synonyms:methoxy(5-(4-(N,N-dimethylamino)phenyl)ethynyl-10,15-diphenylsubporphyrinato)boron(III)

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Chemical Property of methoxy(5-(4-(N,N-dimethylamino)phenyl)ethynyl-10,15-diphenylsubporphyrinato)boron(III)

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Technology Process of methoxy(5-(4-(N,N-dimethylamino)phenyl)ethynyl-10,15-diphenylsubporphyrinato)boron(III)

There total 7 articles about methoxy(5-(4-(N,N-dimethylamino)phenyl)ethynyl-10,15-diphenylsubporphyrinato)boron(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1392132-04-5
methoxo(5-bromo-10,15-diphenylsubporphyrinato)boron(III)

: 17573-94-3,752235-18-0
4-ethynyl-N,N-dimethylaniline

: 1392132-11-4
methoxy(5-(4-(N,N-dimethylamino)phenyl)ethynyl-10,15-diphenylsubporphyrinato)boron(III)

Guidance literature:: With copper(l) iodide; bis(triphenylphosphine)palladium(II) chloride; diisopropylamine; In toluene; at 80 ℃; for 12h; Inert atmosphere;
DOI:10.1002/anie.201201853

Reference yield:

: 195381-16-9
5,10-diphenyltripyrrane

: 1392132-11-4
methoxy(5-(4-(N,N-dimethylamino)phenyl)ethynyl-10,15-diphenylsubporphyrinato)boron(III)

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1,2-dichloro-benzene / 2 h / 150 °C / Inert atmosphere

2.1: 1,2-dichloro-benzene / 1 h / 100 °C

2.2: air / 1 h / Reflux

3.1: N-Bromosuccinimide / chloroform / 0.25 h / 0 °C

4.1: copper(l) iodide; bis(triphenylphosphine)palladium(II) chloride; diisopropylamine / toluene / 12 h / 80 °C / Inert atmosphere

With N-Bromosuccinimide; copper(l) iodide; bis(triphenylphosphine)palladium(II) chloride; diisopropylamine; In chloroform; 1,2-dichloro-benzene; toluene; 4.1: Sonogashira coupling;
DOI:10.1002/anie.201201853

Reference yield:

: 1392132-03-4
methoxo(5,10-diphenylsubporphyrinato)boron(III)

: 1392132-11-4
methoxy(5-(4-(N,N-dimethylamino)phenyl)ethynyl-10,15-diphenylsubporphyrinato)boron(III)

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide / chloroform / 0.25 h / 0 °C

2: copper(l) iodide; bis(triphenylphosphine)palladium(II) chloride; diisopropylamine / toluene / 12 h / 80 °C / Inert atmosphere

With N-Bromosuccinimide; copper(l) iodide; bis(triphenylphosphine)palladium(II) chloride; diisopropylamine; In chloroform; toluene; 2: Sonogashira coupling;
DOI:10.1002/anie.201201853