N',N-didodecyl-Nα-[(3-(N'''-benzyloxycarbonyl)amino)propanoyl]-L-glutamide

Base Information

Chemical Name:N',N-didodecyl-Nα-[(3-(N'''-benzyloxycarbonyl)amino)propanoyl]-L-glutamide
CAS No.:111682-03-2
Molecular Formula:C₄₀H₇₀N₄O₅
Molecular Weight:687.02
Hs Code.:

Synonyms:N',N-didodecyl-Nα-[(3-(N'''-benzyloxycarbonyl)amino)propanoyl]-L-glutamide

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Chemical Property of N',N-didodecyl-Nα-[(3-(N'''-benzyloxycarbonyl)amino)propanoyl]-L-glutamide

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Technology Process of N',N-didodecyl-Nα-[(3-(N'''-benzyloxycarbonyl)amino)propanoyl]-L-glutamide

There total 5 articles about N',N-didodecyl-Nα-[(3-(N'''-benzyloxycarbonyl)amino)propanoyl]-L-glutamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 2304-94-1
3-(benzyloxycarbonylamino)propanoic acid

: 35088-96-1
(S)-2-amino-N₁,N₅-didodecylpentanediamide

: 111682-03-2
N',N-didodecyl-Nα-[(3-(N'''-benzyloxycarbonyl)amino)propanoyl]-L-glutamide

Guidance literature:: With diethyl cyanophosphonate; triethylamine; In tetrahydrofuran; at 20 ℃; for 24h;
DOI:10.1039/b305928f

Reference yield:

: 110766-25-1
N¹,N⁵-didodecyl-N²-benzyloxycarbonyl-L-glutamide

: 111682-03-2
N',N-didodecyl-Nα-[(3-(N'''-benzyloxycarbonyl)amino)propanoyl]-L-glutamide

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / hydrogen / Pd / dimethylformamide / 8 h / 40 °C

2: 93 percent / triethyamine; diethyl cyanophosphate / tetrahydrofuran / 24 h / 20 °C

With diethyl cyanophosphonate; hydrogen; triethylamine; palladium; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/b305928f

Reference yield:

: 124-22-1
n-Dodecylamine

: 111682-03-2
N',N-didodecyl-Nα-[(3-(N'''-benzyloxycarbonyl)amino)propanoyl]-L-glutamide

Guidance literature:: Multi-step reaction with 3 steps

1: 51 percent / triethylamine; diethyl cyanophosphate / tetrahydrofuran / 6.5 h / 0 - 20 °C

2: 68 percent / hydrogen / Pd / dimethylformamide / 8 h / 40 °C

3: 93 percent / triethyamine; diethyl cyanophosphate / tetrahydrofuran / 24 h / 20 °C

With diethyl cyanophosphonate; hydrogen; triethylamine; palladium; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/b305928f