C₁₀H₈Cl₂O₂

Base Information

Chemical Name:C₁₀H₈Cl₂O₂
CAS No.:1252030-78-6
Molecular Formula:C₁₀H₈Cl₂O₂
Molecular Weight:231.078
Hs Code.:

C<sub>10</sub>H<sub>8</sub>Cl<sub>2</sub>O<sub>2</sub>

Synonyms:C₁₀H₈Cl₂O₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₀H₈Cl₂O₂

Chemical Property:

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Technology Process of C₁₀H₈Cl₂O₂

There total 4 articles about C₁₀H₈Cl₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 959749-03-2
5-chloro-2-cyclopropoxybenzoic acid

: 1252030-78-6
C₁₀H₈Cl₂O₂

Guidance literature:: With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 959749-02-1
Methyl 5-chloro-2-cyclopropoxybenzoate

: 1252030-78-6
C₁₀H₈Cl₂O₂

Guidance literature:: Methyl 5-chloro-2-cyclopropoxybenzoate; With sodium hydroxide; In tetrahydrofuran; water; at 60 ℃; for 1h;

With thionyl chloride; In tetrahydrofuran; water; for 4h; Reflux;
DOI:10.1016/j.bmcl.2019.04.008

Reference yield:

: 4068-78-4
methyl 5-chloro-2-hydroxybenzoate

: 1252030-78-6
C₁₀H₈Cl₂O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 16 h / 70 °C

2.1: potassium tert-butylate / tetrahydrofuran / 0 °C

3.1: diethylzinc; trifluoroacetic acid / dichloromethane; hexane / 8 h / 0 - 25 °C

4.1: sodium hydroxide / tetrahydrofuran; water / 1 h / 60 °C

4.2: 4 h / Reflux

With potassium tert-butylate; diethylzinc; caesium carbonate; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; hexane; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2019.04.008