N₆-benzoyl-5'-(tert-butyldimethylsilyl)-3'-(methyl phosphonyl) 2'-deoxyadenosine triethylammonium salt

Base Information

• Chemical Name: N₆-benzoyl-5'-(tert-butyldimethylsilyl)-3'-(methyl phosphonyl) 2'-deoxyadenosine triethylammonium salt
• CAS No.: 1162656-05-4
• Molecular Formula: C₆H₁₅N*C₂₄H₃₄N₅O₆PSi
• Molecular Weight: 648.815

Synonyms:N₆-benzoyl-5'-(tert-butyldimethylsilyl)-3'-(methyl phosphonyl) 2'-deoxyadenosine triethylammonium salt

Chemical Property of N₆-benzoyl-5'-(tert-butyldimethylsilyl)-3'-(methyl phosphonyl) 2'-deoxyadenosine triethylammonium salt

Chemical Property:

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Technology Process of N₆-benzoyl-5'-(tert-butyldimethylsilyl)-3'-(methyl phosphonyl) 2'-deoxyadenosine triethylammonium salt

There total 1 articles about N₆-benzoyl-5'-(tert-butyldimethylsilyl)-3'-(methyl phosphonyl) 2'-deoxyadenosine triethylammonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

methylphosphonic acid (993-13-5) + N6-benzoyl-5′-O-(tert-butyldimethylsilyl)-2′-deoxyadenosine (51549-39-4) + triethylamine (121-44-8) → N6-benzoyl-5'-(tert-butyldimethylsilyl)-3'-(methyl phosphonyl) 2'-deoxyadenosine triethylammonium salt (1162656-05-4)

Guidance literature:

methylphosphonic acid; N⁶-benzoyl-5′-O-(tert-butyldimethylsilyl)-2′-deoxyadenosine; With pyridine; dicyclohexyl-carbodiimide; at 20 ℃; for 48h;

triethylamine; In methanol; dichloromethane;

DOI:10.1016/j.bmc.2009.03.028

upstream raw materials:

methylphosphonic acid

N⁶-benzoyl-5′-O-(tert-butyldimethylsilyl)-2′-deoxyadenosine

triethylamine

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