C₁₃H₁₇NO₂

Base Information

Chemical Name:C₁₃H₁₇NO₂
CAS No.:1221231-88-4
Molecular Formula:C₁₃H₁₇NO₂
Molecular Weight:219.283
Hs Code.:

C<sub>13</sub>H<sub>17</sub>NO<sub>2</sub>

Synonyms:C₁₃H₁₇NO₂

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Chemical Property of C₁₃H₁₇NO₂

Chemical Property:

Purity/Quality:

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Technology Process of C₁₃H₁₇NO₂

There total 1 articles about C₁₃H₁₇NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17206-61-0
hept-6-enal

: 586-96-9
Nitrosobenzene

: 1221231-88-4
C₁₃H₁₇NO₂

Guidance literature:: Nitrosobenzene; With D-Prolin; In chloroform; at 0 ℃; for 0.25h; Inert atmosphere;

hept-6-enal; In chloroform; for 3h; Inert atmosphere;
DOI:10.1021/ja903790y

Reference yield:

: 1221231-88-4
C₁₃H₁₇NO₂

: 1173892-97-1
(-)-(S)-2-(N-phenyl-aminooxy)-hept-6-en-1-ol

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 ℃; for 0.5h; optical yield given as %ee; Inert atmosphere;
DOI:10.1021/ja903790y

Reference yield:

: 1221231-88-4
C₁₃H₁₇NO₂

: C₃₀H₃₇NO₇

Guidance literature:: Multi-step reaction with 23 steps

1.1: sodium tetrahydroborate / methanol / 0.5 h / 0 °C / Inert atmosphere

2.1: acetic acid; zinc / ethanol / 2 h / 23 °C / Inert atmosphere

3.1: 1H-imidazole; dmap / N,N-dimethyl-formamide / 3 h / 0 °C / Inert atmosphere

4.1: Proton Sponge_.(R). / dichloromethane / 3 h / 23 °C / Inert atmosphere; Molecular sieve

5.1: hydrogenchloride / methanol / 0.25 h / 23 °C / Inert atmosphere

6.1: pyridine-SO₃ complex; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.25 h / 23 °C / Inert atmosphere

7.1: triphenylphosphine / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

7.2: 0 °C / Inert atmosphere

8.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; thallium(I) carbonate / tetrahydrofuran; water / 10 h / 23 °C / Inert atmosphere; Darkness

9.1: copper(l) iodide; potassium carbonate; N,N`-dimethylethylenediamine / toluene / 23 - 120 °C / Inert atmosphere

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 23 °C / Inert atmosphere

11.1: pyridine-SO₃ complex; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.25 h / 23 °C / Inert atmosphere

12.1: triethylamine / dichloromethane / 2 h / -78 °C / Inert atmosphere

13.1: Hoveyda-Grubbs catalyst second generation / dichloromethane / 1 h / 23 °C / Inert atmosphere

14.1: 2,6-di-tert-butyl-4-methyl-phenol; N,N-diethylaniline / acetonitrile / 7 h / 95 °C / Inert atmosphere

15.1: titanium tetrachloride / dichloromethane / 0.03 h / -78 °C / Inert atmosphere; Molecular sieve

16.1: Martins sulfurane / benzene / 0.5 h / 23 °C / Inert atmosphere

17.1: n-butyllithium / tetrahydrofuran; hexane / -78 - 0 °C / Inert atmosphere

17.2: -78 - -40 °C / Inert atmosphere

17.3: -78 - -10 °C / Inert atmosphere

18.1: sodium tetrahydroborate / ethanol / 0.5 h / 0 °C / Inert atmosphere

19.1: potassium carbonate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran; water / 0 °C / Inert atmosphere

20.1: water; toluene-4-sulfonic acid / benzene / 23 °C / Inert atmosphere

21.1: trichlorophosphate / 0.5 h / 0 °C / Inert atmosphere

21.2: 0 - 23 °C / Inert atmosphere

22.1: silica gel; 2,3-dicyano-5,6-dichloro-p-benzoquinone / water; acetonitrile / 6 h / 23 °C / Inert atmosphere

23.1: sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 23 °C / Inert atmosphere

With 1H-imidazole; hydrogenchloride; dmap; sodium chlorite; sodium tetrahydroborate; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; Hoveyda-Grubbs catalyst second generation; thallium(I) carbonate; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; Martins sulfurane; pyridine-SO₃ complex; 2,6-di-tert-butyl-4-methyl-phenol; tetrabutyl ammonium fluoride; water; silica gel; titanium tetrachloride; potassium carbonate; toluene-4-sulfonic acid; acetic acid; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; N,N-diethylaniline; 2,3-dicyano-5,6-dichloro-p-benzoquinone; N,N`-dimethylethylenediamine; zinc; trichlorophosphate; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; tert-butyl alcohol; benzene; 8.1: Suzuki coupling / 14.1: Diels-Alder reaction;
DOI:10.1021/ja903790y