Technology Process of C24H20ClFN2O7
There total 15 articles about C24H20ClFN2O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine;
In
acetonitrile;
at 0 - 20 ℃;
for 2.5h;
- Guidance literature:
-
Multi-step reaction with 10 steps
1.1: pyridine / 20 °C
2.1: silver nitrate; 2,4,6-trimethyl-pyridine / dichloromethane / 20 °C
2.2: 20 °C
3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C
4.1: pyridine; Dess-Martin periodane / dichloromethane / 4 h / 0 - 20 °C
4.2: 20 °C
5.1: pyridine / dichloromethane / 0.83 h / -35 °C
6.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 - 20 °C
7.1: lithium chloride / 2 h
8.1: sodium hydroxide / tetrahydrofuran; water / 1 h / 20 °C
9.1: formic acid / 20 °C
10.1: pyridine / acetonitrile / 2.5 h / 0 - 20 °C
With
pyridine; 2,4,6-trimethyl-pyridine; formic acid; tetrabutyl ammonium fluoride; sodium hydride; Dess-Martin periodane; silver nitrate; lithium chloride; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: silver nitrate; 2,4,6-trimethyl-pyridine / dichloromethane / 20 °C
1.2: 20 °C
2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C
3.1: pyridine; Dess-Martin periodane / dichloromethane / 4 h / 0 - 20 °C
3.2: 20 °C
4.1: pyridine / dichloromethane / 0.83 h / -35 °C
5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 - 20 °C
5.2: 2 h
5.3: 1 h / 20 °C
6.1: formic acid / 20 °C
7.1: pyridine / acetonitrile / 2.5 h / 0 - 20 °C
With
pyridine; 2,4,6-trimethyl-pyridine; formic acid; tetrabutyl ammonium fluoride; sodium hydride; Dess-Martin periodane; silver nitrate;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile; mineral oil;