(R)-2-Benzyloxycarbonylamino-4-(2-tert-butoxycarbonylamino-ethylsulfamoyl)-butyric acid benzyl ester

Base Information

Chemical Name:(R)-2-Benzyloxycarbonylamino-4-(2-tert-butoxycarbonylamino-ethylsulfamoyl)-butyric acid benzyl ester
CAS No.:152983-19-2
Molecular Formula:C₂₆H₃₅N₃O₈S
Molecular Weight:549.645
Hs Code.:

Synonyms:(R)-2-Benzyloxycarbonylamino-4-(2-tert-butoxycarbonylamino-ethylsulfamoyl)-butyric acid benzyl ester

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Chemical Property of (R)-2-Benzyloxycarbonylamino-4-(2-tert-butoxycarbonylamino-ethylsulfamoyl)-butyric acid benzyl ester

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Technology Process of (R)-2-Benzyloxycarbonylamino-4-(2-tert-butoxycarbonylamino-ethylsulfamoyl)-butyric acid benzyl ester

There total 2 articles about (R)-2-Benzyloxycarbonylamino-4-(2-tert-butoxycarbonylamino-ethylsulfamoyl)-butyric acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 69164-71-2
(RS)-2-(benzyloxycarbonylamino)-4-(chlorosulfonyl)butanoic acid benzyl ester

: 79513-35-2,117083-06-4
N-(tert-butyloxycarbonyl)-1,2-ethanediamine hydrochloride

: 152871-77-7
(S)-2-Benzyloxycarbonylamino-4-(2-tert-butoxycarbonylamino-ethylsulfamoyl)-butyric acid

: 152983-19-2
(R)-2-Benzyloxycarbonylamino-4-(2-tert-butoxycarbonylamino-ethylsulfamoyl)-butyric acid benzyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 ℃; for 1h; Yield given. Title compound not separated from byproducts;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 152983-19-2
(R)-2-Benzyloxycarbonylamino-4-(2-tert-butoxycarbonylamino-ethylsulfamoyl)-butyric acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / 1N NaOH (phenolphthalein) / H₂O; propan-2-ol / 24 h / Ambient temperature

2: 100 percent / DIPEA / dimethylformamide / 1 h / 0 °C

With sodium hydroxide; N-ethyl-N,N-diisopropylamine; In water; N,N-dimethyl-formamide; isopropyl alcohol;