5-(benzyloxycarbonylaminopentyl) 3,4,6-tri-O-acetyl-2-chloroacetamido-2-deoxy-β-D-glucopyranose

Base Information

Chemical Name:5-(benzyloxycarbonylaminopentyl) 3,4,6-tri-O-acetyl-2-chloroacetamido-2-deoxy-β-D-glucopyranose
CAS No.:160242-92-2
Molecular Formula:C₂₇H₃₇ClN₂O₁₁
Molecular Weight:601.051
Hs Code.:

Synonyms:5-(benzyloxycarbonylaminopentyl) 3,4,6-tri-O-acetyl-2-chloroacetamido-2-deoxy-β-D-glucopyranose

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Chemical Property of 5-(benzyloxycarbonylaminopentyl) 3,4,6-tri-O-acetyl-2-chloroacetamido-2-deoxy-β-D-glucopyranose

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Technology Process of 5-(benzyloxycarbonylaminopentyl) 3,4,6-tri-O-acetyl-2-chloroacetamido-2-deoxy-β-D-glucopyranose

There total 1 articles about 5-(benzyloxycarbonylaminopentyl) 3,4,6-tri-O-acetyl-2-chloroacetamido-2-deoxy-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 87905-98-4
5-<(benzyloxycarbonyl)amino>pentanol

: 68499-56-9
1,3,4,6-tetra-O-acetyl-2-chloroacetamido-2-deoxy-β-D-glucopyranoside

: 160242-92-2
5-(benzyloxycarbonylaminopentyl) 3,4,6-tri-O-acetyl-2-chloroacetamido-2-deoxy-β-D-glucopyranose

Guidance literature:: With 3 A molecular sieve; iron(III) chloride; In dichloromethane; for 3h;
DOI:10.1016/0008-6215(94)84179-9

Reference yield: 94.0%

: 160242-92-2
5-(benzyloxycarbonylaminopentyl) 3,4,6-tri-O-acetyl-2-chloroacetamido-2-deoxy-β-D-glucopyranose

: 87906-01-2
5-(benzyloxycarbonylaminopentyl) 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: With acetic acid; zinc; for 1h; Ambient temperature;
DOI:10.1016/0008-6215(94)84179-9

Reference yield:

: 160242-92-2
5-(benzyloxycarbonylaminopentyl) 3,4,6-tri-O-acetyl-2-chloroacetamido-2-deoxy-β-D-glucopyranose

: 87906-05-6
5-(benzyloxycarbonylamino)pentyl 2-acetamido-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / Zn, AcOH / 1 h / Ambient temperature

2: 96 percent / NaOMe / methanol / 24 h / Ambient temperature

With sodium methylate; acetic acid; zinc; In methanol;
DOI:10.1016/0008-6215(94)84179-9